Technology Process of C25H26BNO7
There total 4 articles about C25H26BNO7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C30H35BO6;
With
sodium hydroxide;
In
tetrahydrofuran; water;
for 0.25h;
nitromethane;
In
tetrahydrofuran; water;
at 20 ℃;
for 15h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 90 °C
2.1: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / N,N-dimethyl-formamide / 14 h / 90 °C / Inert atmosphere
3.1: sodium hydroxide / water; tetrahydrofuran / 0.25 h
3.2: 15 h / 20 °C
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate; potassium carbonate; sodium hydroxide;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / N,N-dimethyl-formamide / 14 h / 90 °C / Inert atmosphere
2.1: sodium hydroxide / water; tetrahydrofuran / 0.25 h
2.2: 15 h / 20 °C
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate; sodium hydroxide;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;