lithium salt of 6-benzyl-4-hydroxy-6-aza-spiro[2.5]oct-4-ene-5-carboxylic acid tert-butyl ester

Base Information

Chemical Name:lithium salt of 6-benzyl-4-hydroxy-6-aza-spiro[2.5]oct-4-ene-5-carboxylic acid tert-butyl ester
CAS No.:1101840-78-1
Molecular Formula:C₁₉H₂₄NO₃*Li
Molecular Weight:321.345
Hs Code.:

Synonyms:lithium salt of 6-benzyl-4-hydroxy-6-aza-spiro[2.5]oct-4-ene-5-carboxylic acid tert-butyl ester

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Chemical Property of lithium salt of 6-benzyl-4-hydroxy-6-aza-spiro[2.5]oct-4-ene-5-carboxylic acid tert-butyl ester

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Technology Process of lithium salt of 6-benzyl-4-hydroxy-6-aza-spiro[2.5]oct-4-ene-5-carboxylic acid tert-butyl ester

There total 1 articles about lithium salt of 6-benzyl-4-hydroxy-6-aza-spiro[2.5]oct-4-ene-5-carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1101840-76-9
1-[2-(benzyl-tert-butoxycarbonylmethyl-amino)-ethyl]-cyclopropanecarboxylic acid tert-butyl ester

: 1101840-78-1
lithium salt of 6-benzyl-4-hydroxy-6-aza-spiro[2.5]oct-4-ene-5-carboxylic acid tert-butyl ester

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at 20 - 25 ℃; for 4.5h;

Reference yield:

: 1101840-78-1
lithium salt of 6-benzyl-4-hydroxy-6-aza-spiro[2.5]oct-4-ene-5-carboxylic acid tert-butyl ester

: 1101840-77-0
6-benzyl-6-aza-spiro[2.5]octan-4-one hydrochloride

Guidance literature:: lithium salt of 6-benzyl-4-hydroxy-6-aza-spiro[2.5]oct-4-ene-5-carboxylic acid tert-butyl ester; With sulfuric acid; In water; at -10 - 40 ℃;

With sodium hydrogencarbonate; sodium hydroxide; In water; pH=7.4 - 9.4;

With hydrogenchloride; In ethyl acetate; at 0 - 20 ℃;