Technology Process of O-methyl-N-[3-(2,4,6-trichloro-phenyl)-propyl]-hydroxylamine
There total 6 articles about O-methyl-N-[3-(2,4,6-trichloro-phenyl)-propyl]-hydroxylamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-(2,4,6-trichloro-phenyl)-propionaldehyde O-methyl-oxime;
With
sodium cyanoborohydride; acetic acid;
at 0 - 20 ℃;
for 6h;
With
sodium hydroxide;
In
water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: thionyl chloride / 3 h / 110 °C / Reflux
2.1: pyridine / chloroform / 3 h / 0 - 20 °C
3.1: diisobutylaluminium hydride / toluene / 3.33 h / -60 °C
3.2: 0.25 h
4.1: triethylamine / methanol / 2 h / 60 °C
5.1: sodium cyanoborohydride; acetic acid / 6 h / 0 - 20 °C
With
pyridine; thionyl chloride; diisobutylaluminium hydride; sodium cyanoborohydride; acetic acid; triethylamine;
In
methanol; chloroform; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylammonium formate / 0.17 h / 20 °C
1.2: 3 h / 120 °C / Reflux
2.1: thionyl chloride / 3 h / 110 °C / Reflux
3.1: pyridine / chloroform / 3 h / 0 - 20 °C
4.1: diisobutylaluminium hydride / toluene / 3.33 h / -60 °C
4.2: 0.25 h
5.1: triethylamine / methanol / 2 h / 60 °C
6.1: sodium cyanoborohydride; acetic acid / 6 h / 0 - 20 °C
With
pyridine; thionyl chloride; diisobutylaluminium hydride; triethylammonium formate; sodium cyanoborohydride; acetic acid; triethylamine;
In
methanol; chloroform; toluene;
