C₄₂H₆₅N₅O₆

Base Information

• Chemical Name: C₄₂H₆₅N₅O₆
• CAS No.: 1009093-99-5
• Molecular Formula: C₄₂H₆₅N₅O₆
• Molecular Weight: 736.008
• Mol file: 1009093-99-5.mol

Synonyms:C₄₂H₆₅N₅O₆

Chemical Property of C₄₂H₆₅N₅O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₂H₆₅N₅O₆

There total 10 articles about C₄₂H₆₅N₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

C40H61N5O6 (1009093-91-7) + acetaldehyde (75-07-0,9002-91-9) → C42H65N5O6 (1009093-99-5)

Guidance literature:

With sodium cyanoborohydride; In methanol; at 20 ℃;

Reference yield:

C8H10INO2 (874347-50-9) → C42H65N5O6 (1009093-99-5)

Guidance literature:

Multi-step reaction with 7 steps

1.1: benzene / Heating / reflux

2.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

2.2: 2 h

3.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C

4.1: trimethylaluminum / hexane; dichloromethane / 0.25 h

4.2: 20 °C

4.3: 2 h

5.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 36 h / 60 °C

6.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide

7.1: sodium cyanoborohydride / methanol / 20 °C

With titanium(IV) isopropylate; trimethylaluminum; potassium acetate; sodium cyanoborohydride; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; benzene;

Reference yield:

C11H12INO4 (1009091-77-3) → C42H65N5O6 (1009093-99-5)

Guidance literature:

Multi-step reaction with 6 steps

1.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

1.2: 2 h

2.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C

3.1: trimethylaluminum / hexane; dichloromethane / 0.25 h

3.2: 20 °C

3.3: 2 h

4.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 36 h / 60 °C

5.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide

6.1: sodium cyanoborohydride / methanol / 20 °C

With titanium(IV) isopropylate; trimethylaluminum; potassium acetate; sodium cyanoborohydride; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

upstream raw materials:

C₄₀H₆₁N₅O₆

acetaldehyde

C₈H₁₀INO₂

C₁₁H₁₂INO₄