Technology Process of C18H24O2
There total 4 articles about C18H24O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C18H26O3;
With
methanesulfonyl chloride; triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
With
sodium hydroxide;
tetra(n-butyl)ammonium hydrogensulfate;
at 20 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl acetamide / 6 h / 100 °C
2.1: potassium hydroxide / water; methanol / 40 °C / Reflux
3.1: triethylamine; methanesulfonyl chloride / dichloromethane / 0 - 20 °C
3.2: 4 h / 20 °C
With
potassium carbonate; methanesulfonyl chloride; triethylamine; potassium hydroxide;
In
methanol; dichloromethane; N,N-dimethyl acetamide; water;
2.1: Aldol-Cannizzaro Reaction;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydroxide / water; methanol / 40 °C / Reflux
2.1: triethylamine; methanesulfonyl chloride / dichloromethane / 0 - 20 °C
2.2: 4 h / 20 °C
With
methanesulfonyl chloride; triethylamine; potassium hydroxide;
In
methanol; dichloromethane; water;
1.1: Aldol-Cannizzaro Reaction;