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Technology Process of 2Pd(2+)*4C6H9(CH3)(NC)C(CH3)2NC*Br(1-)*3ClO4(1-)=Pd2[C6H9(CH3)(NC)C(CH3)2NC]4Br(ClO4)3

2Pd(2+)*4C6H9(CH3)(NC)C(CH3)2NC*Br(1-)*3ClO4(1-)=Pd2[C6H9(CH3)(NC)C(CH3)2NC]4Br(ClO4)3

Base Information
  • Chemical Name:2Pd(2+)*4C6H9(CH3)(NC)C(CH3)2NC*Br(1-)*3ClO4(1-)=Pd2[C6H9(CH3)(NC)C(CH3)2NC]4Br(ClO4)3
  • CAS No.:90839-45-5
  • Molecular Formula:Br*4C12H18N2*3ClO4*2Pd
  • Molecular Weight:1352.25
  • Hs Code.:
2Pd<sup>(2+)</sup>*4C<sub>6</sub>H<sub>9</sub>(CH<sub>3</sub>)(NC)C(CH<sub>3</sub>)2NC*Br<sup>(1-)</sup>*3ClO<sub>4</sub><sup>(1-)</sup>=Pd<sub>2</sub>[C<sub>6</sub>H<sub>9</sub>(CH<sub>3</sub>)(NC)C(CH<sub>3</sub>)2NC]4Br(ClO<sub>4</sub>)3

Synonyms:2Pd(2+)*4C6H9(CH3)(NC)C(CH3)2NC*Br(1-)*3ClO4(1-)=Pd2[C6H9(CH3)(NC)C(CH3)2NC]4Br(ClO4)3

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Chemical Property of 2Pd(2+)*4C6H9(CH3)(NC)C(CH3)2NC*Br(1-)*3ClO4(1-)=Pd2[C6H9(CH3)(NC)C(CH3)2NC]4Br(ClO4)3
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Technology Process of 2Pd(2+)*4C6H9(CH3)(NC)C(CH3)2NC*Br(1-)*3ClO4(1-)=Pd2[C6H9(CH3)(NC)C(CH3)2NC]4Br(ClO4)3

There total 1 articles about 2Pd(2+)*4C6H9(CH3)(NC)C(CH3)2NC*Br(1-)*3ClO4(1-)=Pd2[C6H9(CH3)(NC)C(CH3)2NC]4Br(ClO4)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

bis(acetonitrile)palladium(II) bromide
920282-22-0,53623-19-1

bis(acetonitrile)palladium(II) bromide

1,8-di-isocyano-p-menthane
86469-90-1

1,8-di-isocyano-p-menthane

2Pd<sup>(2+)</sup>*4C<sub>6</sub>H<sub>9</sub>(CH<sub>3</sub>)(NC)C(CH<sub>3</sub>)2NC*Br<sup>(1-)</sup>*3ClO<sub>4</sub><sup>(1-)</sup>=Pd<sub>2</sub>[C<sub>6</sub>H<sub>9</sub>(CH<sub>3</sub>)(NC)C(CH<sub>3</sub>)2NC]4Br(ClO<sub>4</sub>)3
90839-45-5

2Pd(2+)*4C6H9(CH3)(NC)C(CH3)2NC*Br(1-)*3ClO4(1-)=Pd2[C6H9(CH3)(NC)C(CH3)2NC]4Br(ClO4)3

Guidance literature:
With LiClO4; In methanol; slow addn. of ligand to Pd-complex suspension, addn. of LiClO4 to soln.obtained (sometimes after filtration); standing, pptn., filtration, washing (MeOH-ether 1:5), drying (vac., room temp.); elem. anal.;
upstream raw materials:

bis(acetonitrile)palladium(II) bromide

1,8-di-isocyano-p-menthane

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