((4-(tert-butyl)phenyl)ethynyl)triisopropylsilane

Base Information

Chemical Name:((4-(tert-butyl)phenyl)ethynyl)triisopropylsilane
CAS No.:945773-25-1
Molecular Formula:C₂₁H₃₄Si
Molecular Weight:314.586
Hs Code.:

Synonyms:((4-(tert-butyl)phenyl)ethynyl)triisopropylsilane

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Chemical Property of ((4-(tert-butyl)phenyl)ethynyl)triisopropylsilane

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Technology Process of ((4-(tert-butyl)phenyl)ethynyl)triisopropylsilane

There total 7 articles about ((4-(tert-butyl)phenyl)ethynyl)triisopropylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 35779-04-5
1-tert-butyl-4-iodobenzene

: 89343-06-6
tris-iso-propylsilyl acetylene

: 945773-25-1
((4-(tert-butyl)phenyl)ethynyl)triisopropylsilane

Guidance literature:: With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; at 20 ℃; for 21h;
DOI:10.1016/j.tet.2007.05.019

Reference yield: 90.0%

: 89343-06-6
tris-iso-propylsilyl acetylene

: 4-(tert-butyl)benzoyl fluoride

: 945773-25-1
((4-(tert-butyl)phenyl)ethynyl)triisopropylsilane

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; tributyl-amine; 1,3-bis-(diphenylphosphino)propane; In 1,4-dioxane; at 140 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1055/s-0040-1705954

Reference yield: 86.0%

: 1-(4-(tert-butyl)benzoyl)piperidine-2,6-dione

: 89343-06-6
tris-iso-propylsilyl acetylene

: 945773-25-1
((4-(tert-butyl)phenyl)ethynyl)triisopropylsilane

Guidance literature:: 1-(4-(tert-butyl)benzoyl)piperidine-2,6-dione; With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; copper(l) iodide; 1,2-bis-(dicyclohexylphosphino)ethane; In 1,4-dioxane; at 20 ℃; for 0.0833333h; Glovebox;

tris-iso-propylsilyl acetylene; In 1,4-dioxane; at 150 ℃; for 16h; Sealed tube;
DOI:10.1021/acs.orglett.7b01194