(R)-(4-dimethylaminophenyl)methoxycarbonylaminoacetic acid methyl ester

Base Information

Chemical Name:(R)-(4-dimethylaminophenyl)methoxycarbonylaminoacetic acid methyl ester
CAS No.:444997-80-2
Molecular Formula:C₁₃H₁₈N₂O₄
Molecular Weight:266.297
Hs Code.:

Synonyms:(R)-(4-dimethylaminophenyl)methoxycarbonylaminoacetic acid methyl ester

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Chemical Property of (R)-(4-dimethylaminophenyl)methoxycarbonylaminoacetic acid methyl ester

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Technology Process of (R)-(4-dimethylaminophenyl)methoxycarbonylaminoacetic acid methyl ester

There total 1 articles about (R)-(4-dimethylaminophenyl)methoxycarbonylaminoacetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 786589-52-4
[(E)-Methoxycarbonylimino]-acetic acid methyl ester

: 444997-80-2
(R)-(4-dimethylaminophenyl)methoxycarbonylaminoacetic acid methyl ester

Guidance literature:: With tetrakis(acetonitrile)copper(I) hexafluorophosphate; (R)-2,2'-bis[bis(3-methylphenyl)phosphino]-1,1'-binaphthyl; In tetrahydrofuran; toluene; at -78 ℃; for 24h;
DOI:10.1021/jo0256787

Reference yield: 84.0%

: 444997-80-2
(R)-(4-dimethylaminophenyl)methoxycarbonylaminoacetic acid methyl ester

: amino-(4-dimethylaminophenyl)acetic acid methyl ester

Guidance literature:: (R)-(4-dimethylaminophenyl)methoxycarbonylaminoacetic acid methyl ester; With trimethylsilyl iodide; In acetonitrile; at 60 ℃; for 0.75h;

With methanol; at 20 ℃; for 0.333333h; Further stages.;
DOI:10.1021/jo0256787

Reference yield: 78.0%

: 444997-80-2
(R)-(4-dimethylaminophenyl)methoxycarbonylaminoacetic acid methyl ester

: 444997-85-7
(4-aminophenyl)methoxycarbonylaminoacetic acid methyl ester

Guidance literature:: (R)-(4-dimethylaminophenyl)methoxycarbonylaminoacetic acid methyl ester; With trimethylsilylazide; iodosylbenzene; In dichloromethane; at -40 ℃; for 3h;

With sodium hydrogencarbonate; In tetrahydrofuran; at 20 ℃; for 48h; Further stages.;
DOI:10.1021/jo0256787