benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-α-D-galactopyranosyl)-2-deoxy-α-D-galactopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-α-D-galactopyranosyl)-2-deoxy-α-D-galactopyranoside
CAS No.:197795-15-6
Molecular Formula:C₂₃H₃₄N₂O₁₁
Molecular Weight:514.53
Hs Code.:

Synonyms:benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-α-D-galactopyranosyl)-2-deoxy-α-D-galactopyranoside

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Chemical Property of benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-α-D-galactopyranosyl)-2-deoxy-α-D-galactopyranoside

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Technology Process of benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-α-D-galactopyranosyl)-2-deoxy-α-D-galactopyranoside

There total 5 articles about benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-α-D-galactopyranosyl)-2-deoxy-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: N-[(2S,3R,4R,5R,6R)-4-((2S,3R,4R,5R,6R)-3-Azido-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-2-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl]-acetamide

: 197795-15-6
benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-α-D-galactopyranosyl)-2-deoxy-α-D-galactopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 16 - 48 ℃; for 24h; Yield given;

Reference yield:

: 3554-91-4
Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

: 197795-15-6
benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-α-D-galactopyranosyl)-2-deoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Ag₂CO₃, AgClO₄, 4 Angstroem sieves / 1.) CH₂Cl₂, RT, 1 h, 2.) CH₂Cl₂, RT, 24 h

2: aq. AcOH / 70 - 80 °C

3: NaOMe / methanol

4: H₂ / 10percent Pd/C / methanol / 24 h / 16 - 48 °C

With 4 A molecular sieve; hydrogen; sodium methylate; silver perchlorate; acetic acid; silver carbonate; palladium on activated charcoal; In methanol;

Reference yield:

: 67817-37-2
3,4,6-tri-O-acetyl-2-azido-2-deoxy-β-D-galactopyranosyl chloride

: 197795-15-6
benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-α-D-galactopyranosyl)-2-deoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Ag₂CO₃, AgClO₄, 4 Angstroem sieves / 1.) CH₂Cl₂, RT, 1 h, 2.) CH₂Cl₂, RT, 24 h

2: aq. AcOH / 70 - 80 °C

3: NaOMe / methanol

4: H₂ / 10percent Pd/C / methanol / 24 h / 16 - 48 °C

With 4 A molecular sieve; hydrogen; sodium methylate; silver perchlorate; acetic acid; silver carbonate; palladium on activated charcoal; In methanol;