4-[1-methyl-1-(N-methyl-N-phenylcarbamoyl)ethylcarbamoyl]-3,3-dimethylbutyl acetate

Base Information

Chemical Name:4-[1-methyl-1-(N-methyl-N-phenylcarbamoyl)ethylcarbamoyl]-3,3-dimethylbutyl acetate
CAS No.:884877-05-8
Molecular Formula:C₂₀H₃₀N₂O₄
Molecular Weight:362.469
Hs Code.:

Synonyms:4-[1-methyl-1-(N-methyl-N-phenylcarbamoyl)ethylcarbamoyl]-3,3-dimethylbutyl acetate

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Chemical Property of 4-[1-methyl-1-(N-methyl-N-phenylcarbamoyl)ethylcarbamoyl]-3,3-dimethylbutyl acetate

Chemical Property:

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Technology Process of 4-[1-methyl-1-(N-methyl-N-phenylcarbamoyl)ethylcarbamoyl]-3,3-dimethylbutyl acetate

There total 3 articles about 4-[1-methyl-1-(N-methyl-N-phenylcarbamoyl)ethylcarbamoyl]-3,3-dimethylbutyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 884877-04-7
5-acetoxy-3,3-dimethylpentanoic acid

: 75755-40-7
2,2-dimethyl-3-(N-methyl-N-phenylamino)-2H-azirine

: 884877-05-8
4-[1-methyl-1-(N-methyl-N-phenylcarbamoyl)ethylcarbamoyl]-3,3-dimethylbutyl acetate

Guidance literature:: In tetrahydrofuran; at 20 ℃;
DOI:10.1002/hlca.200690038

Reference yield:

: 22791-80-6
4,4-dimethyl-tetrahydro-pyran-2-one

: 884877-05-8
4-[1-methyl-1-(N-methyl-N-phenylcarbamoyl)ethylcarbamoyl]-3,3-dimethylbutyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH / methanol; H₂O / 2 h / 20 °C

2: 1201 mg / 14 h / 80 °C

3: 86 percent / tetrahydrofuran / 20 °C

With sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1002/hlca.200690038

Reference yield:

: 156089-56-4
5-hydroxy-3,3-dimethyl-valeric acid

: 884877-05-8
4-[1-methyl-1-(N-methyl-N-phenylcarbamoyl)ethylcarbamoyl]-3,3-dimethylbutyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1201 mg / 14 h / 80 °C

2: 86 percent / tetrahydrofuran / 20 °C

In tetrahydrofuran;
DOI:10.1002/hlca.200690038