(3aS,7aR)-3a-Hydroxy-4-[2-(3-methoxy-phenyl)-ethyl]-7a-methyl-hexahydro-indene-1,5-dione

Base Information

Chemical Name:(3aS,7aR)-3a-Hydroxy-4-[2-(3-methoxy-phenyl)-ethyl]-7a-methyl-hexahydro-indene-1,5-dione
CAS No.:96789-74-1
Molecular Formula:C₁₉H₂₄O₄
Molecular Weight:316.397
Hs Code.:

Synonyms:(3aS,7aR)-3a-Hydroxy-4-[2-(3-methoxy-phenyl)-ethyl]-7a-methyl-hexahydro-indene-1,5-dione

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Chemical Property of (3aS,7aR)-3a-Hydroxy-4-[2-(3-methoxy-phenyl)-ethyl]-7a-methyl-hexahydro-indene-1,5-dione

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Technology Process of (3aS,7aR)-3a-Hydroxy-4-[2-(3-methoxy-phenyl)-ethyl]-7a-methyl-hexahydro-indene-1,5-dione

There total 5 articles about (3aS,7aR)-3a-Hydroxy-4-[2-(3-methoxy-phenyl)-ethyl]-7a-methyl-hexahydro-indene-1,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 96728-44-8
4-<2'-(m-methoxyphenyl)ethyl>-7a-methyl-4a,2'-oxyindan-3,7-dione

: 96789-74-1
(3aS,7aR)-3a-Hydroxy-4-[2-(3-methoxy-phenyl)-ethyl]-7a-methyl-hexahydro-indene-1,5-dione

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 60 ℃; for 2h; under 760 Torr;
DOI:10.1021/jo00216a034

Reference yield:

: 119087-33-1
3-Bromo-1-[2-(3-methoxy-phenyl)-cyclopropyl]-propan-1-one

: 96789-74-1
(3aS,7aR)-3a-Hydroxy-4-[2-(3-methoxy-phenyl)-ethyl]-7a-methyl-hexahydro-indene-1,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 76.4 percent / acetonitrile / Ambient temperature

2: 81 percent / SnCl₄ / CH₂Cl₂ / Ambient temperature

3: 75 percent / H₂ / 10percent Pd/C / ethanol / 2 h / 60 °C / 760 Torr

With hydrogen; tin(IV) chloride; palladium on activated charcoal; In ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jo00216a034

Reference yield:

: 51467-21-1
Sodium salt of 2-Methyl-1,3-cyclopentadione

: 96789-74-1
(3aS,7aR)-3a-Hydroxy-4-[2-(3-methoxy-phenyl)-ethyl]-7a-methyl-hexahydro-indene-1,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 76.4 percent / acetonitrile / Ambient temperature

2: 81 percent / SnCl₄ / CH₂Cl₂ / Ambient temperature

3: 75 percent / H₂ / 10percent Pd/C / ethanol / 2 h / 60 °C / 760 Torr

With hydrogen; tin(IV) chloride; palladium on activated charcoal; In ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jo00216a034