(2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-4-benzylpiperidinylamide

Base Information

Chemical Name:(2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-4-benzylpiperidinylamide
CAS No.:368443-77-0
Molecular Formula:C₃₁H₃₂N₂O₅
Molecular Weight:512.605
Hs Code.:

Synonyms:(2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-4-benzylpiperidinylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-4-benzylpiperidinylamide

Chemical Property:

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Technology Process of (2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-4-benzylpiperidinylamide

There total 4 articles about (2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-4-benzylpiperidinylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 368443-76-9
4-(4-benzyl-piperidin-1-yl)-3-(9H-fluoren-9-ylmethoxycarbonylamino)-4-oxo-butyric acid allyl ester

: 368443-77-0
(2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-4-benzylpiperidinylamide

Guidance literature:: With phenylsilane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1039/b100401h

Reference yield:

: 31252-42-3
4-benzylpyperidine

: 368443-77-0
(2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-4-benzylpiperidinylamide

Guidance literature:: Multi-step reaction with 2 steps

1: NMM / tetrahydrofuran / 4 h / 0 - 20 °C

2: 700 mg / PhSiH₃ / (Ph₃P)4Pd⁽⁰⁾ / CH₂Cl₂ / 18 h / 20 °C

With 4-methyl-morpholine; phenylsilane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b100401h

Reference yield:

: 177609-12-0
N-alpha-(9-fluorenylmethyloxycarbonyl)-D-aspartic acid beta-allyl ester

: 368443-77-0
(2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartic α-4-benzylpiperidinylamide

Guidance literature:: Multi-step reaction with 3 steps

1: NMM / tetrahydrofuran / 0.08 h / -15 °C

2: NMM / tetrahydrofuran / 4 h / 0 - 20 °C

3: 700 mg / PhSiH₃ / (Ph₃P)4Pd⁽⁰⁾ / CH₂Cl₂ / 18 h / 20 °C

With 4-methyl-morpholine; phenylsilane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b100401h