methyl 2,4,6-tri-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-α/β-D-glucopyranosyl)-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,4,6-tri-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-α/β-D-glucopyranosyl)-α-D-glucopyranoside
CAS No.:92812-57-2
Molecular Formula:C₆₂H₆₆O₁₁
Molecular Weight:987.199
Hs Code.:

Synonyms:methyl 2,4,6-tri-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-α/β-D-glucopyranosyl)-α-D-glucopyranoside

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Chemical Property of methyl 2,4,6-tri-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-α/β-D-glucopyranosyl)-α-D-glucopyranoside

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Technology Process of methyl 2,4,6-tri-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-α/β-D-glucopyranosyl)-α-D-glucopyranoside

There total 28 articles about methyl 2,4,6-tri-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-α/β-D-glucopyranosyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 35303-86-7
(2R,3S,4S,5R,6S)-3,5-Bis-benzyloxy-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-4-ol

: 1H-indol-2-yl 2,3,4,6-tetra-O-benzyl-1-thio-α-D-glucopyranoside

: 92812-57-2
methyl 2,4,6-tri-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-α/β-D-glucopyranosyl)-α-D-glucopyranoside

: 64694-19-5
methyl 2,3,4,6-tetra-O-benzyl-D-glucopyranosyl-α-(1→3)-2,4,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: (2R,3S,4S,5R,6S)-3,5-Bis-benzyloxy-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-4-ol; 1H-indol-2-yl 2,3,4,6-tetra-O-benzyl-1-thio-α-D-glucopyranoside; In dichloromethane; at 20 ℃; for 1h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; silver carbonate; In dichloromethane; at -70 - 20 ℃; Overall yield = 70 percent; stereoselective reaction; Inert atmosphere;
DOI:10.1021/acs.joc.0c00943

Reference yield:

: C₃₇H₃₄Co₂O₁₂

: 131531-76-5
p-methylphenyl 2,3,4,6-tetra-O-benzyl-thio-β-D-glucopyranoside

: 92812-57-2
methyl 2,4,6-tri-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-α/β-D-glucopyranosyl)-α-D-glucopyranoside

: 64694-19-5
methyl 2,3,4,6-tetra-O-benzyl-D-glucopyranosyl-α-(1→3)-2,4,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; Overall yield = 69 %; Inert atmosphere;
DOI:10.1016/j.tetlet.2017.05.012