2-allyloxymethyl-3-oxa-1,6-hexanediol ditosylate

Base Information

Chemical Name:2-allyloxymethyl-3-oxa-1,6-hexanediol ditosylate
CAS No.:187839-70-9
Molecular Formula:C₂₃H₃₀O₈S₂
Molecular Weight:498.618
Hs Code.:

Synonyms:2-allyloxymethyl-3-oxa-1,6-hexanediol ditosylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-allyloxymethyl-3-oxa-1,6-hexanediol ditosylate

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Technology Process of 2-allyloxymethyl-3-oxa-1,6-hexanediol ditosylate

There total 3 articles about 2-allyloxymethyl-3-oxa-1,6-hexanediol ditosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 98-59-9
p-toluenesulfonyl chloride

: 187839-69-6
2-allyloxymethyl-3-oxa-1,6-hexanediol

: 187839-70-9
2-allyloxymethyl-3-oxa-1,6-hexanediol ditosylate

Guidance literature:: With pyridine; at 0 - 5 ℃; for 3h;
DOI:10.1002/jhet.5570330672

Reference yield:

: 95870-54-5
1-O-allyl-3-O-triphenylmethylglycerol

: 187839-70-9
2-allyloxymethyl-3-oxa-1,6-hexanediol ditosylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, 0.5 h, 2.) DMF, from 60 to 70 deg C, 24 h

2: aq. HCl / methanol; CH₂Cl₂ / 48 h / 30 - 35 °C

3: 80 percent / pyridine / 3 h / 0 - 5 °C

With pyridine; hydrogenchloride; sodium hydride; In methanol; dichloromethane;
DOI:10.1002/jhet.5570330672

Reference yield:

: 187839-68-5
C₄₇H₄₆O₄

: 187839-70-9
2-allyloxymethyl-3-oxa-1,6-hexanediol ditosylate

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / methanol; CH₂Cl₂ / 48 h / 30 - 35 °C

2: 80 percent / pyridine / 3 h / 0 - 5 °C

With pyridine; hydrogenchloride; In methanol; dichloromethane;
DOI:10.1002/jhet.5570330672