benzyl (S)-N-phthaloyltryptophanyl-(S)-prolinate

Base Information

• Chemical Name: benzyl (S)-N-phthaloyltryptophanyl-(S)-prolinate
• CAS No.: 883556-44-3
• Molecular Formula: C₃₁H₂₇N₃O₅
• Molecular Weight: 521.572

Synonyms:benzyl (S)-N-phthaloyltryptophanyl-(S)-prolinate

Chemical Property of benzyl (S)-N-phthaloyltryptophanyl-(S)-prolinate

Chemical Property:

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Technology Process of benzyl (S)-N-phthaloyltryptophanyl-(S)-prolinate

There total 1 articles about benzyl (S)-N-phthaloyltryptophanyl-(S)-prolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N-phthalimide-L-tryptophan (32675-71-1,48208-26-0,62361-30-2) + H-Pro-OBzl (41324-66-7) → benzyl (S)-N-phthaloyltryptophanyl-(S)-prolinate (883556-44-3)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 13h;

DOI:10.1021/ol060016f

Reference yield: 77.0%

benzyl (S)-N-phthaloyltryptophanyl-(S)-prolinate (883556-44-3) + 1H-imidazole (288-32-4) → benzyl (S)-[N-phthaloyl-2-(N-1-imidazolyl)tryptophanyl]-(S)-prolinate

Guidance literature:

With N,N'-dimethylpiperazine; N-chloro-succinimide; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1021/ol060016f

Reference yield: 58.0%

benzyl (S)-N-phthaloyltryptophanyl-(S)-prolinate (883556-44-3) + Nα-benzyloxycarbonyl-NG-(2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl)-L-arginyl-L-histidine tert-butyl ester (883556-49-8) → C68H76N10O13S (883556-51-2)

Guidance literature:

With N,N'-dimethylpiperazine; N-chloro-succinimide; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1021/ol060016f

upstream raw materials:

N-phthalimide-L-tryptophan

H-Pro-OBzl

Downstream raw materials:

C₆₈H₇₆N₁₀O₁₃S

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