5-cyclopentyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine

Base Information

Chemical Name:5-cyclopentyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine
CAS No.:1043927-66-7
Molecular Formula:C₃₁H₃₃N₃O₅S
Molecular Weight:559.686
Hs Code.:

Synonyms:5-cyclopentyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine

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Chemical Property of 5-cyclopentyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine

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Technology Process of 5-cyclopentyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine

There total 1 articles about 5-cyclopentyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1043871-02-8
3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanic acid

: 1043927-65-6
5-cyclopentyl-2,3-dihydro-[1H]-2-benzazepine

: 1043927-66-7
5-cyclopentyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine

Guidance literature:: 3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

5-cyclopentyl-2,3-dihydro-[1H]-2-benzazepine; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1039/b801206g

Reference yield: 91.0%

: 1043927-66-7
5-cyclopentyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine

: 5-cyclopentyl-4,5-dihydroxy-2-[3-N-(2-nitrophenylsulfonyl)-N-(phenylmethyl)amino]propanoyl-2,3,4,5-tetrahydro-[1H]-2-benzazepine

Guidance literature:: With osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; In acetone; tert-butyl alcohol; at 20 ℃; for 16h;
DOI:10.1039/b801206g