2-hydroxy-1,1-dimethyl-2,2-bis-(p-tolyl)ethyl t-butyl sulphoxide

Base Information

Chemical Name:2-hydroxy-1,1-dimethyl-2,2-bis-(p-tolyl)ethyl t-butyl sulphoxide
CAS No.:78752-72-4
Molecular Formula:C₂₂H₃₀O₂S
Molecular Weight:358.545
Hs Code.:

Synonyms:2-hydroxy-1,1-dimethyl-2,2-bis-(p-tolyl)ethyl t-butyl sulphoxide

Suppliers and Price of 2-hydroxy-1,1-dimethyl-2,2-bis-(p-tolyl)ethyl t-butyl sulphoxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxy-1,1-dimethyl-2,2-bis-(p-tolyl)ethyl t-butyl sulphoxide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of 2-hydroxy-1,1-dimethyl-2,2-bis-(p-tolyl)ethyl t-butyl sulphoxide

There total 2 articles about 2-hydroxy-1,1-dimethyl-2,2-bis-(p-tolyl)ethyl t-butyl sulphoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 611-97-2
bis(p-methylphenyl)-methanone

: 25432-21-7
isopropyl t-butyl sulphoxide

: 78752-72-4
2-hydroxy-1,1-dimethyl-2,2-bis-(p-tolyl)ethyl t-butyl sulphoxide

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.0833333h;
DOI:10.1039/P19810001826

Reference yield:

: 44657-76-3
2-methyl-2-[(1-methylethyl)thio]-propane

: 78752-72-4
2-hydroxy-1,1-dimethyl-2,2-bis-(p-tolyl)ethyl t-butyl sulphoxide

Guidance literature:: Multi-step reaction with 2 steps

1: m-ClC₆H₄CO₃H / ethyl acetate / 48 h / Ambient temperature

2: 51 percent / n-BuLi / tetrahydrofuran / 0.08 h / -78 °C

With n-butyllithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethyl acetate;
DOI:10.1039/P19810001826

Reference yield:

: 78752-72-4
2-hydroxy-1,1-dimethyl-2,2-bis-(p-tolyl)ethyl t-butyl sulphoxide

: 4399-34-2
2-methyl-1,1-bis-(p-tolyl)prop-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: SO₂Cl₂ / CH₂Cl₂ / 1.) -78 deg C, 30 min, 2.) -78 deg C -> 0 deg C

2: CDCl₃ / 15 h / 12 °C

With sulfuryl dichloride; In chloroform-d1; dichloromethane;
DOI:10.1039/P19810001826