methyl 3-azido-3-deoxy-2-O-mesyl-5-O-triphenylmethyl-β-D-xylofuranoside

Base Information

Chemical Name:methyl 3-azido-3-deoxy-2-O-mesyl-5-O-triphenylmethyl-β-D-xylofuranoside
CAS No.:923600-33-3
Molecular Formula:C₂₆H₂₇N₃O₆S
Molecular Weight:509.583
Hs Code.:

Synonyms:methyl 3-azido-3-deoxy-2-O-mesyl-5-O-triphenylmethyl-β-D-xylofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-azido-3-deoxy-2-O-mesyl-5-O-triphenylmethyl-β-D-xylofuranoside

Chemical Property:

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Technology Process of methyl 3-azido-3-deoxy-2-O-mesyl-5-O-triphenylmethyl-β-D-xylofuranoside

There total 2 articles about methyl 3-azido-3-deoxy-2-O-mesyl-5-O-triphenylmethyl-β-D-xylofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 923600-32-2
methyl 2,3-di-O-mesyl-5-O-trityl-β-D-ribofuranoside

: 923600-33-3
methyl 3-azido-3-deoxy-2-O-mesyl-5-O-triphenylmethyl-β-D-xylofuranoside

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 110 ℃; for 43h;
DOI:10.1080/10426500500326545

Reference yield:

: 50908-04-8
(-)-Methyl-5-O-trityl-β-D-ribofuranosid

: 923600-33-3
methyl 3-azido-3-deoxy-2-O-mesyl-5-O-triphenylmethyl-β-D-xylofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 84.6 percent / pyridine / 66 h / 20 °C

2: 34 percent / NaN₃ / dimethylformamide / 43 h / 110 °C

With pyridine; sodium azide; In N,N-dimethyl-formamide;
DOI:10.1080/10426500500326545