N-(p-anisyl)-4-methylbenzenecarboxyimidoyl chloride

Base Information

• Chemical Name: N-(p-anisyl)-4-methylbenzenecarboxyimidoyl chloride
• CAS No.: 84662-52-2
• Molecular Formula: C₁₅H₁₄ClNO
• Molecular Weight: 259.735
• Mol file: 84662-52-2.mol

Synonyms:N-(p-anisyl)-4-methylbenzenecarboxyimidoyl chloride

Chemical Property of N-(p-anisyl)-4-methylbenzenecarboxyimidoyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(p-anisyl)-4-methylbenzenecarboxyimidoyl chloride

There total 3 articles about N-(p-anisyl)-4-methylbenzenecarboxyimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N-(4-methoxyphenyl)-4-methylbenzamide (33667-91-3) → N-(p-anisyl)-4-methylbenzenecarboxyimidoyl chloride (84662-52-2)

Guidance literature:

With thionyl chloride; at 80 ℃;

DOI:10.1002/adsc.200700466

Reference yield:

4-methyl-benzoyl chloride (874-60-2) → N-(p-anisyl)-4-methylbenzenecarboxyimidoyl chloride (84662-52-2)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / ethyl acetate / 0 - 10 °C

2: thionyl chloride / Reflux

With thionyl chloride; triethylamine; In ethyl acetate;

DOI:10.1002/jhet.1031

Reference yield:

p-Toluic acid (99-94-5) → N-(p-anisyl)-4-methylbenzenecarboxyimidoyl chloride (84662-52-2)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride / Reflux

2: triethylamine / ethyl acetate / 0 - 10 °C

3: thionyl chloride / Reflux

With thionyl chloride; triethylamine; In ethyl acetate;

DOI:10.1002/jhet.1031

upstream raw materials:

N-(4-methoxyphenyl)-4-methylbenzamide

4-methyl-benzoyl chloride

p-Toluic acid

Downstream raw materials:

diethyl α-(p-anisylimino)-4-methylbenzylphosphonate

4-(4-methoxyphenyl)-3-(4-nitrophenyl)-5-p-tolyl-4H-[1,2,4]triazole

4-[4-(4-methoxyphenyl)-5-p-tolyl-4H-[1,2,4]triazol-3-yl]pyridine