Technology Process of C47H52F4N8O6SSi
There total 8 articles about C47H52F4N8O6SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 90 percent / K2CO3 / methanol
2: 85 percent / HBTU; DIPEA / CH2Cl2
3: Ph3P; DEAD / tetrahydrofuran
With
potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; dichloromethane;
3: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2007.05.009
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 85 percent / HBTU; DIPEA / CH2Cl2
2: Ph3P; DEAD / tetrahydrofuran
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane;
2: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2007.05.009
- Guidance literature:
-
Multi-step reaction with 6 steps
1: TFA / CH2Cl2
2: methanol
3: 75 percent / BF3*Et2O / CH2Cl2
4: 90 percent / K2CO3 / methanol
5: 85 percent / HBTU; DIPEA / CH2Cl2
6: Ph3P; DEAD / tetrahydrofuran
With
boron trifluoride diethyl etherate; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; dichloromethane;
6: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2007.05.009
