tert-butyl [2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol]uronate

Base Information

Chemical Name:tert-butyl [2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol]uronate
CAS No.:1207750-78-4
Molecular Formula:C₃₀H₃₄N₂O₉S
Molecular Weight:598.674
Hs Code.:

Synonyms:tert-butyl [2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol]uronate

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Chemical Property of tert-butyl [2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol]uronate

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Technology Process of tert-butyl [2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol]uronate

There total 1 articles about tert-butyl [2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol]uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1207750-77-3
tert-butyl [2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-4-O-(1-naphthyl)methyl-N-(4-nitro)benzenesulfonyl-L-iditol]uronate

: 1207750-78-4
tert-butyl [2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol]uronate

Guidance literature:: With ammonium cerium (IV) nitrate; In water; acetonitrile; at 20 ℃; for 3h;
DOI:10.1016/j.tetlet.2009.11.042

Reference yield: 90.0%

: 1207750-80-8
phenyl 2-azido-3,4-di-O-benzyl-6-O-chloroacetyl-2-deoxy-1-thio-α,β-D-glucopyranoside

: 1207750-78-4
tert-butyl [2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol]uronate

: 1207750-82-0
(2-azido-3,4-di-O-benzyl-2-deoxy-6-O-chloroacetyl-α-D-glucopyranosyl)-(1->4)-[tert-butyl [2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol]uronate]

Guidance literature:: phenyl 2-azido-3,4-di-O-benzyl-6-O-chloroacetyl-2-deoxy-1-thio-α,β-D-glucopyranoside; tert-butyl [2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol]uronate; In diethyl ether; dichloromethane; at -30 ℃; for 1h; Molecular sieve; Inert atmosphere;

With Me₂S₂-Tf₂O; In diethyl ether; dichloromethane; for 0.0833333h; stereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.tetlet.2009.11.042