exo-1-(phenylacetoxy)-9-phenyl-cis-bicyclo<6.2.0>decan-10-one

Base Information

• Chemical Name: exo-1-(phenylacetoxy)-9-phenyl-cis-bicyclo<6.2.0>decan-10-one
• CAS No.: 122898-98-0
• Molecular Formula: C₂₄H₂₆O₃
• Molecular Weight: 362.469
• Mol file: 122898-98-0.mol

Synonyms:exo-1-(phenylacetoxy)-9-phenyl-cis-bicyclo<6.2.0>decan-10-one

Chemical Property of exo-1-(phenylacetoxy)-9-phenyl-cis-bicyclo<6.2.0>decan-10-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of exo-1-(phenylacetoxy)-9-phenyl-cis-bicyclo<6.2.0>decan-10-one

There total 3 articles about exo-1-(phenylacetoxy)-9-phenyl-cis-bicyclo<6.2.0>decan-10-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

phenylacetic acid (103-82-2) + 9-chloro-9-phenylbicyclo<6.2.0>decan-10-one (122923-84-6) → exo-1-(phenylacetoxy)-9-phenyl-cis-bicyclo<6.2.0>decan-10-one (122898-98-0)

Guidance literature:

With triethylamine; In acetone; at 20 ℃;

DOI:10.1021/jo00281a045

Reference yield:

cis-Cyclooctene (931-88-4,931-87-3,25267-51-0) → exo-1-(phenylacetoxy)-9-phenyl-cis-bicyclo<6.2.0>decan-10-one (122898-98-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / triethylamine / 0.5 h / 70 - 80 °C

2: 86 percent / triethylamine / acetone / 20 °C

With triethylamine; In acetone;

DOI:10.1021/jo00281a045

Reference yield:

α-chlorophenylacetyl chloride (2912-62-1) → exo-1-(phenylacetoxy)-9-phenyl-cis-bicyclo<6.2.0>decan-10-one (122898-98-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / triethylamine / 0.5 h / 70 - 80 °C

2: 86 percent / triethylamine / acetone / 20 °C

With triethylamine; In acetone;

DOI:10.1021/jo00281a045

upstream raw materials:

phenylacetic acid

9-chloro-9-phenylbicyclo<6.2.0>decan-10-one

cis-Cyclooctene

α-chlorophenylacetyl chloride