C₁₈H₁₈O₃

Base Information

• Chemical Name: C₁₈H₁₈O₃
• CAS No.: 1217666-27-7
• Molecular Formula: C₁₈H₁₈O₃
• Molecular Weight: 282.339
• Mol file: 1217666-27-7.mol

Synonyms:C₁₈H₁₈O₃

Chemical Property of C₁₈H₁₈O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₈H₁₈O₃

There total 1 articles about C₁₈H₁₈O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

divinylketone (1890-28-4) + C13H11IO2 (1217666-23-3) → C18H18O3 (1217666-27-7)

Guidance literature:

C₁₃H₁₁IO₂; With isopropylmagnesium chloride; In tetrahydrofuran; diethyl ether; pentane; at -30 - 0 ℃;

divinylketone; With N,N,N,N,N,N-hexamethylphosphoric triamide; chloro-trimethyl-silane; copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; diethyl ether; pentane; at -78 - 18 ℃; for 17.5h;

With water; ammonium chloride; at 18 ℃; for 0.166667h;

DOI:10.1039/b921600f

Reference yield: 59.0%

C18H18O3 (1217666-27-7) → C18H18O3 (1217666-37-9) + C18H18O3 (1217666-39-1)

Guidance literature:

With 2,6-di-tert-butyl-4-methyl-phenol; In toluene; for 24h; Reflux;

DOI:10.1039/b921600f

upstream raw materials:

divinylketone

C₁₃H₁₁IO₂

Downstream raw materials:

C₁₈H₁₈O₃

C₁₈H₁₈O₃

Refernces