6,7-dichloro-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazo[4,5-b]quinolin-2-thione

Base Information

• Chemical Name: 6,7-dichloro-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazo[4,5-b]quinolin-2-thione
• CAS No.: 285132-09-4
• Molecular Formula: C₃₆H₂₅Cl₂N₃O₇S
• Molecular Weight: 714.582

Synonyms:6,7-dichloro-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazo[4,5-b]quinolin-2-thione

Chemical Property of 6,7-dichloro-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazo[4,5-b]quinolin-2-thione

Chemical Property:

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Technology Process of 6,7-dichloro-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazo[4,5-b]quinolin-2-thione

There total 2 articles about 6,7-dichloro-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazo[4,5-b]quinolin-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C38H26Cl2N6O7 → 6,7-dichloro-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazo[4,5-b]quinolin-2-thione (285132-09-4)

Guidance literature:

With hydrogen sulfide; triethylamine; In acetonitrile; at 20 ℃; for 0.5h;

DOI:10.1021/jm990290y

Reference yield:

6,7-dichloro-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazo<4,5-b>quinolin-2-one (177980-41-5) → 6,7-dichloro-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazo[4,5-b]quinolin-2-thione (285132-09-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: POCl₃ / acetonitrile / 20 °C

1.2: Et₃N / acetonitrile / 24 h / 20 °C

2.1: H₂S; Et₃N / acetonitrile / 0.5 h / 20 °C

With hydrogen sulfide; triethylamine; trichlorophosphate; In acetonitrile; 1.1: Phosphorylation / 1.2: Condensation / 2.1: Substitution;

DOI:10.1021/jm990290y

Reference yield:

6,7-dichloro-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazo[4,5-b]quinolin-2-thione (285132-09-4) → C36H24Cl3N3O7 (1053714-57-0)

Guidance literature:

With tetrachloromethane; chlorine; In dichloromethane; at -78 ℃; for 2h;

DOI:10.1021/jm990290y

upstream raw materials:

6,7-dichloro-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazo<4,5-b>quinolin-2-one

Downstream raw materials:

C₃₆H₂₄Cl₃N₃O₇

2-benzylthio-6,7-dichloro-1-(β-D-ribofuranosyl)imidazo[4,5-b]quinoline

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