C₁₄H₁₉N₃O₃S

Base Information

• Chemical Name: C₁₄H₁₉N₃O₃S
• CAS No.: 1071983-07-7
• Molecular Formula: C₁₄H₁₉N₃O₃S
• Molecular Weight: 309.389
• Mol file: 1071983-07-7.mol

Synonyms:C₁₄H₁₉N₃O₃S

Chemical Property of C₁₄H₁₉N₃O₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₁₉N₃O₃S

There total 3 articles about C₁₄H₁₉N₃O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

N-acetyl-penicillamine benzylamide → C14H19N3O3S (1071983-07-7)

Guidance literature:

With hydrogenchloride; sulfuric acid; sodium nitrite; In methanol; water; at 5 ℃; for 1h; Darkness;

DOI:10.1039/C8CC08868C

Reference yield:

L-penicillamine (1113-41-3) → C14H19N3O3S (1071983-07-7)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / 20 h / 20 °C

2: chloroform / 24 h / 20 °C

3: hydrogenchloride; sulfuric acid; sodium nitrite / methanol; water / 1 h / 5 °C / Darkness

With pyridine; hydrogenchloride; sulfuric acid; sodium nitrite; In methanol; chloroform; water;

DOI:10.1039/C8CC08868C

Reference yield:

(3R)-3-acetamido-4,4-dimethylthietan-2-one (88168-59-6) → C14H19N3O3S (1071983-07-7)

Guidance literature:

Multi-step reaction with 2 steps

1: chloroform / 24 h / 20 °C

2: hydrogenchloride; sulfuric acid; sodium nitrite / methanol; water / 1 h / 5 °C / Darkness

With hydrogenchloride; sulfuric acid; sodium nitrite; In methanol; chloroform; water;

DOI:10.1039/C8CC08868C

upstream raw materials:

L-penicillamine

(3R)-3-acetamido-4,4-dimethylthietan-2-one

Downstream raw materials:

C₃₃H₃₄N₃O₄PS