methyl 5-O-(2,3-anhydro-β-L-lyxofuranosyl)-2,3-di-O-benzyl-α-L-arabinofuranoside

Base Information

Chemical Name:methyl 5-O-(2,3-anhydro-β-L-lyxofuranosyl)-2,3-di-O-benzyl-α-L-arabinofuranoside
CAS No.:527682-23-1
Molecular Formula:C₂₅H₃₀O₈
Molecular Weight:458.508
Hs Code.:

Synonyms:methyl 5-O-(2,3-anhydro-β-L-lyxofuranosyl)-2,3-di-O-benzyl-α-L-arabinofuranoside

Suppliers and Price of methyl 5-O-(2,3-anhydro-β-L-lyxofuranosyl)-2,3-di-O-benzyl-α-L-arabinofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 5-O-(2,3-anhydro-β-L-lyxofuranosyl)-2,3-di-O-benzyl-α-L-arabinofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 5-O-(2,3-anhydro-β-L-lyxofuranosyl)-2,3-di-O-benzyl-α-L-arabinofuranoside

There total 9 articles about methyl 5-O-(2,3-anhydro-β-L-lyxofuranosyl)-2,3-di-O-benzyl-α-L-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Benzoic acid (1R,2S,4S,5R)-4-((2S,3S,4R,5R)-3,4-bis-benzyloxy-5-methoxy-tetrahydro-furan-2-ylmethoxy)-3,6-dioxa-bicyclo[3.1.0]hex-2-ylmethyl ester

: 527682-23-1
methyl 5-O-(2,3-anhydro-β-L-lyxofuranosyl)-2,3-di-O-benzyl-α-L-arabinofuranoside

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 1h;
DOI:10.1021/ja029302m

Reference yield:

: 42793-97-5
2,3,5-tri-O-benzoyl-1-O-methyl-α-L-arabinofuranose

: 527682-23-1
methyl 5-O-(2,3-anhydro-β-L-lyxofuranosyl)-2,3-di-O-benzyl-α-L-arabinofuranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: 100 percent / NaOMe / methanol; CH₂Cl₂ / 6 h / 20 °C

2.1: 81 percent / pyridine

3.1: NaH / dimethylformamide / 0.25 h / 0 °C

3.2: 87 percent / dimethylformamide / 3 h / 0 - 20 °C

4.1: 93 percent / p-TsOH / methanol; CH₂Cl₂ / 6 h / 20 °C

5.1: 4 A molecular sieves; N-iodosuccinimide; silver triflate / CH₂Cl₂ / -40 °C

6.1: NaOMe / methanol / 1 h / 20 °C

With pyridine; N-iodo-succinimide; 4 A molecular sieve; sodium methylate; silver trifluoromethanesulfonate; sodium hydride; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja029302m

Reference yield:

: 16896-03-0
methyl 2,3-di-O-benzyl-α-L-arabinofuranoside

: 527682-23-1
methyl 5-O-(2,3-anhydro-β-L-lyxofuranosyl)-2,3-di-O-benzyl-α-L-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 4 A molecular sieves; N-iodosuccinimide; silver triflate / CH₂Cl₂ / -40 °C

2: NaOMe / methanol / 1 h / 20 °C

With N-iodo-succinimide; 4 A molecular sieve; sodium methylate; silver trifluoromethanesulfonate; In methanol; dichloromethane;
DOI:10.1021/ja029302m