C₂₁H₂₄N₂O₃

Base Information

Chemical Name:C₂₁H₂₄N₂O₃
CAS No.:1374108-92-5
Molecular Formula:C₂₁H₂₄N₂O₃
Molecular Weight:352.433
Hs Code.:

C<sub>21</sub>H<sub>24</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₁H₂₄N₂O₃

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Chemical Property of C₂₁H₂₄N₂O₃

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Technology Process of C₂₁H₂₄N₂O₃

There total 6 articles about C₂₁H₂₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1374108-91-4
C₃₅H₃₆N₂O₃

: 1374108-92-5
C₂₁H₂₄N₂O₃

Guidance literature:: With methanesulfonic acid; at 20 ℃; for 0.333333h; Cooling with ice;

Reference yield:

: 375358-19-3
2-chloroquinoline-7-ol

: 1374108-92-5
C₂₁H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 20 °C / Cooling with ice

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,2-dimethoxyethane / 16 h / 80 °C / Inert atmosphere

3: trifluoroacetic acid / chloroform / 1 h / 20 °C / Cooling with ice

4: acetic acid; 2-picoline borane complex / methanol / 16 h / 20 °C / Cooling with ice

5: methanesulfonic acid / 0.33 h / 20 °C / Cooling with ice

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; methanesulfonic acid; 2-picoline borane complex; di-isopropyl azodicarboxylate; potassium carbonate; acetic acid; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; chloroform; water;

Reference yield:

: 1374108-70-9
C₂₆H₂₄ClNO₃

: 1374108-92-5
C₂₁H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,2-dimethoxyethane / 16 h / 80 °C / Inert atmosphere

2: trifluoroacetic acid / chloroform / 1 h / 20 °C / Cooling with ice

3: acetic acid; 2-picoline borane complex / methanol / 16 h / 20 °C / Cooling with ice

4: methanesulfonic acid / 0.33 h / 20 °C / Cooling with ice

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; methanesulfonic acid; 2-picoline borane complex; potassium carbonate; acetic acid; trifluoroacetic acid; In methanol; 1,2-dimethoxyethane; chloroform; water;