methyl 2-(3-chloro-4-(3-(methylthio)-4-nitro-2-oxoindolin-5-yloxy)phenyl)acetate

Base Information

Chemical Name:methyl 2-(3-chloro-4-(3-(methylthio)-4-nitro-2-oxoindolin-5-yloxy)phenyl)acetate
CAS No.:1080522-63-9
Molecular Formula:C₁₈H₁₅ClN₂O₆S
Molecular Weight:422.846
Hs Code.:

Synonyms:methyl 2-(3-chloro-4-(3-(methylthio)-4-nitro-2-oxoindolin-5-yloxy)phenyl)acetate

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Chemical Property of methyl 2-(3-chloro-4-(3-(methylthio)-4-nitro-2-oxoindolin-5-yloxy)phenyl)acetate

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Technology Process of methyl 2-(3-chloro-4-(3-(methylthio)-4-nitro-2-oxoindolin-5-yloxy)phenyl)acetate

There total 4 articles about methyl 2-(3-chloro-4-(3-(methylthio)-4-nitro-2-oxoindolin-5-yloxy)phenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4455-13-4
methylthioacetic acid ethyl ester

: C₁₅H₁₃ClN₂O₅

: 1080522-63-9
methyl 2-(3-chloro-4-(3-(methylthio)-4-nitro-2-oxoindolin-5-yloxy)phenyl)acetate

Guidance literature:: C₁₅H₁₃ClN₂O₅; With tert-butylhypochlorite; In dichloromethane; at -65 ℃; for 0.0833333h;

methylthioacetic acid ethyl ester; In dichloromethane; at -65 ℃; for 1h;

With triethylamine; In dichloromethane; at -65 - 25 ℃;

Reference yield:

: 60397-70-8
2-(4-chloro-3-hydroxyphenyl)acetic acid

: 1080522-63-9
methyl 2-(3-chloro-4-(3-(methylthio)-4-nitro-2-oxoindolin-5-yloxy)phenyl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / dimethyl sulfoxide / 16 h / 80 °C

1.2: pH < 4

2.1: methanol; diethyl ether; benzene / 1 h / 25 °C

3.1: tert-butylhypochlorite / dichloromethane / 0.08 h / -65 °C

3.2: 1 h / -65 °C

3.3: -65 - 25 °C

With tert-butylhypochlorite; caesium carbonate; In methanol; diethyl ether; dichloromethane; dimethyl sulfoxide; benzene;

Reference yield:

: 1080521-64-7
2-(4-(4-amino-2-nitrophenoxy)-3-chlorophenyl)acetic acid

: 1080522-63-9
methyl 2-(3-chloro-4-(3-(methylthio)-4-nitro-2-oxoindolin-5-yloxy)phenyl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol; diethyl ether; benzene / 1 h / 25 °C

2.1: tert-butylhypochlorite / dichloromethane / 0.08 h / -65 °C

2.2: 1 h / -65 °C

2.3: -65 - 25 °C

With tert-butylhypochlorite; In methanol; diethyl ether; dichloromethane; benzene;