6-acetyl-10-methylisoalloxazine

Base Information

• Chemical Name: 6-acetyl-10-methylisoalloxazine
• CAS No.: 92642-15-4
• Molecular Formula: C₁₃H₁₀N₄O₃
• Molecular Weight: 270.247
• Mol file: 92642-15-4.mol

Synonyms:6-acetyl-10-methylisoalloxazine

Chemical Property of 6-acetyl-10-methylisoalloxazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 6-acetyl-10-methylisoalloxazine

There total 1 articles about 6-acetyl-10-methylisoalloxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Acetamidoacetophenone (7463-31-2) → 6-acetyl-10-methylisoalloxazine (92642-15-4)

Guidance literature:

Multi-step reaction with 6 steps

1: nitric acid, acetic anhydride

2: KOH / ethanol; H₂O

3: 85 percent / trifluoroacetic anhydride / 0.42 h

4: 92 percent / KOH / acetone / 0.5 h / Heating

5: hydrogen / 10percent palladium on charcoal / ethanol / 2 h

6: 498 mg / ethanol; HCl / 1.) 50-60 deg C, 70 min; 2.) reflux, 15 min

With potassium hydroxide; hydrogen; nitric acid; acetic anhydride; trifluoroacetic anhydride; palladium on activated charcoal; In hydrogenchloride; ethanol; water; acetone;

DOI:10.1021/ja00334a053

upstream raw materials:

3-Acetamidoacetophenone

Refernces