[methoxy-13C,D₃,imido-13C]methyl 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoate

Base Information

• Chemical Name: [methoxy-13C,D₃,imido-13C]methyl 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoate
• CAS No.: 1130037-37-4
• Molecular Formula: C₁₆H₁₃ClFNO₄
• Molecular Weight: 342.689

Synonyms:[methoxy-13C,D₃,imido-13C]methyl 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoate

Chemical Property of [methoxy-13C,D₃,imido-13C]methyl 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoate

Chemical Property:

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Technology Process of [methoxy-13C,D₃,imido-13C]methyl 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoate

There total 1 articles about [methoxy-13C,D₃,imido-13C]methyl 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[carbonyl-13C]2-chloro-5-fluorobenzoyl chloride (1130037-35-2) + [methoxy-13C,D3]methyl 4-amino-3-methoxybenzoate (1130037-29-4) → [methoxy-13C,D3,imido-13C]methyl 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoate (1130037-37-4)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1002/jlcr.1515

Reference yield: 100.0%

[methoxy-13C,D3,imido-13C]methyl 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoate (1130037-37-4) → [methoxy-13C,D3,amido-13C] 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoic acid (1130037-39-6)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 5h;

DOI:10.1002/jlcr.1515

upstream raw materials:

[carbonyl-13C]2-chloro-5-fluorobenzoyl chloride

[methoxy-13C,D₃]methyl 4-amino-3-methoxybenzoate

Downstream raw materials:

[methoxy-13C,D₃,amido-13C] 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoic acid

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