Technology Process of C70H44
There total 4 articles about C70H44 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
ethanol; water; toluene;
at 90 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene; diethyl ether; dibutyl ether / 6 h / -20 °C
2.1: potassium iodide; acetic acid; sodium hypophosphite monohydrate / 6 h / Reflux
3.1: n-butyllithium / hexane; tetrahydrofuran / -80 °C
3.2: 2 h
3.3: 12 h
4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 12 h / 90 °C
With
n-butyllithium; sodium hypophosphite monohydrate; sodium carbonate; acetic acid; potassium iodide;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; diethyl ether; ethanol; hexane; dibutyl ether; water; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / hexane; tetrahydrofuran / -80 °C
1.2: 2 h
1.3: 12 h
2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 12 h / 90 °C
With
n-butyllithium; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; hexane; water; toluene;