C₁₀H₁₀ClNO₄

Base Information

Chemical Name:C₁₀H₁₀ClNO₄
CAS No.:1403259-23-3
Molecular Formula:C₁₀H₁₀ClNO₄
Molecular Weight:243.647
Hs Code.:

C<sub>10</sub>H<sub>10</sub>ClNO<sub>4</sub>

Synonyms:C₁₀H₁₀ClNO₄

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Chemical Property of C₁₀H₁₀ClNO₄

Chemical Property:

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Technology Process of C₁₀H₁₀ClNO₄

There total 2 articles about C₁₀H₁₀ClNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1310378-92-7
methyl 5-chloro-2-ethylbenzoate

: 1403258-46-7
methyl 5-chloro-2-ethyl-3-nitrobenzoate

: 1403259-23-3
C₁₀H₁₀ClNO₄

Guidance literature:: methyl 5-chloro-2-ethylbenzoate; With sulfuric acid; nitric acid; In methanol; at -5 - 0 ℃; for 1.25h; Cooling with ethanol-ice;

With thionyl chloride; In methanol; at 0 ℃; for 6h; Inert atmosphere; Reflux;

Reference yield:

: 27007-53-0
methyl-2-bromo-5-chlorobenzoate

: 1403258-46-7
methyl 5-chloro-2-ethyl-3-nitrobenzoate

: 1403259-23-3
C₁₀H₁₀ClNO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine; triphenylphosphine; copper(l) iodide / palladium diacetate / 20 h / 20 - 50 °C / Inert atmosphere

2.1: potassium carbonate / methanol / 1 h / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 20 °C

4.1: nitric acid; sulfuric acid / methanol / 1.25 h / -5 - 0 °C / Cooling with ethanol-ice

4.2: 6 h / 0 °C / Inert atmosphere; Reflux

With copper(l) iodide; sulfuric acid; hydrogen; nitric acid; potassium carbonate; triethylamine; triphenylphosphine; palladium 10% on activated carbon; palladium diacetate; In methanol; ethyl acetate;