2-(2,3-DICHLOROPHENOXY)THIOACETAMIDE

Base Information

• Chemical Name: 2-(2,3-DICHLOROPHENOXY)THIOACETAMIDE
• CAS No.: 115540-88-0
• Molecular Formula: C₈H₇Cl₂NOS
• Molecular Weight: 236.122
• Mol file: 115540-88-0.mol

Synonyms:2-(2,3-DICHLOROPHENOXY)THIOACETAMIDE

Chemical Property of 2-(2,3-DICHLOROPHENOXY)THIOACETAMIDE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.635
• Boiling Point: 370.32°C at 760 mmHg
• PKA: 12.47±0.29(Predicted)
• Flash Point: 177.764°C
• PSA: 67.34000
• Density: 1.453g/cm³
• LogP: 3.35860

Purity/Quality:

98%min ^*data from raw suppliers

2-(2,3-DICHLOROPHENOXY)THIOACETAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(2,3-DICHLOROPHENOXY)THIOACETAMIDE

There total 3 articles about 2-(2,3-DICHLOROPHENOXY)THIOACETAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dichlorophenoxyacetaldehyde → 2,3-dichlorophenoxythioacetamide (115540-88-0)

Guidance literature:

Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride, sodium hydroxide / aq. ethanol; H₂O / Ambient temperature

2: acetic anhydride / Heating

3: hydrogen sulphide gas, triethylamine, pyridine / Ambient temperature

With pyridine; sodium hydroxide; hydrogen sulfide; hydroxylamine hydrochloride; acetic anhydride; triethylamine; In ethanol; water;

Reference yield:

2,3-dichlorophenoxyacetonitrile (39960-01-5) → 2,3-dichlorophenoxythioacetamide (115540-88-0)

Guidance literature:

With pyridine; hydrogen sulfide; triethylamine; Ambient temperature;

Reference yield:

2,3-dichlorophenoxyacetaldoxime → 2,3-dichlorophenoxythioacetamide (115540-88-0)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic anhydride / Heating

2: hydrogen sulphide gas, triethylamine, pyridine / Ambient temperature

With pyridine; hydrogen sulfide; acetic anhydride; triethylamine;

upstream raw materials:

2,3-dichlorophenoxyacetonitrile

Downstream raw materials:

2-(2,3-dichlorophenoxymethyl)-4-(2'-pyrazinyl)thiazole

2-(2,3-dichlorophenoxymethyl)-4-(5'-nitro-2'-furyl)thiazole

Refernces