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Technology Process of 1-

1-
Base Information
  • Chemical Name:1-
  • CAS No.:136163-23-0
  • Molecular Formula:BrH*C20H29Br2NO2
  • Molecular Weight:556.176
  • Hs Code.:
1-<bis(bromomethyl)methyl)-2-cyclohexyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

Synonyms:1-

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 1-
Chemical Property:
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Technology Process of 1-

There total 3 articles about 1-

synthetic route:

Reference yield: 80.0%

1-<bis(hydroxymethyl)methyl>-2-cycloxexyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
747378-28-5

1--2-cycloxexyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

1-<bis(bromomethyl)methyl)-2-cyclohexyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
136163-23-0

1-

Guidance literature:
With phosphorus tribromide; In benzene; for 2h; Heating;

Reference yield:

1-<bis(hydroxymethyl)-methyl>-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
98661-42-8

1--6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

1-<bis(bromomethyl)methyl)-2-cyclohexyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
136163-23-0

1-

Guidance literature:
Multi-step reaction with 2 steps
1: 2.) sodium borohydride / 1.) ethanol, reflux, 10 h, 2.) ethanol, RT
2: 80 percent / PBr3 / benzene / 2 h / Heating
With sodium tetrahydroborate; phosphorus tribromide; In benzene;

Reference yield:

cyclohexanone
108-94-1,11119-77-0,9003-41-2,9075-99-4

cyclohexanone

1-<bis(bromomethyl)methyl)-2-cyclohexyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
136163-23-0

1-

Guidance literature:
Multi-step reaction with 2 steps
1: 2.) sodium borohydride / 1.) ethanol, reflux, 10 h, 2.) ethanol, RT
2: 80 percent / PBr3 / benzene / 2 h / Heating
With sodium tetrahydroborate; phosphorus tribromide; In benzene;
upstream raw materials:

1--2-cycloxexyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

1--6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

cyclohexanone

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