C₂₃H₃₂O₅

Base Information

Chemical Name:C₂₃H₃₂O₅
CAS No.:363140-03-8
Molecular Formula:C₂₃H₃₂O₅
Molecular Weight:388.504
Hs Code.:

C<sub>23</sub>H<sub>32</sub>O<sub>5</sub>

Synonyms:C₂₃H₃₂O₅

Suppliers and Price of C₂₃H₃₂O₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₃H₃₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₃H₃₂O₅

There total 18 articles about C₂₃H₃₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 363140-02-7
C₂₃H₃₄O₄

: 363140-03-8
C₂₃H₃₂O₅

Guidance literature:: With salcomine; oxygen; In N,N-dimethyl-formamide; at 20 ℃; for 5h;
DOI:10.1021/ol016285h

Reference yield:

: 113666-06-1
(-)-(4aR)-1,4a-dimethyl-4,4a,7,8-tetrahydronaphthalene-2,5(3H,6H)-dione

: 363140-03-8
C₂₃H₃₂O₅

Guidance literature:: Multi-step reaction with 18 steps

1.1: 89 percent / p-toluenesulfonic acid / benzene / 2 h / Heating

2.1: H₂; Pd-C; piperidine / 6 h / 20 °C / 7600.51 Torr

2.2: acetic acid / ethanol / 1.5 h / 15 °C

2.3: thionyl chloride; pyridine / CH₂Cl₂ / 1.5 h / 30 °C

3.1: 96 percent / diisobutylaluminum hydride / toluene / 2 h / -78 °C

4.1: 99 percent / sodium borohydride / H₂O; tetrahydrofuran / 0.5 h / 0 °C

5.1: 100 percent / hydrochloric acid / H₂O; methanol / 1 h / 20 °C

6.1: 37 percent / hydroquinone / 1,2-dichloro-benzene / 30 h / 20 - 170 °C

7.1: 96 percent / p-toluenesulfonic acid / benzene / 4 h / Heating

8.1: 77 percent / [Ir(cod)Pcy₃(py)]+PF₆- / CH₂Cl₂ / 48 h / -20 °C

9.1: 100 percent / lithium aluminium hydride / tetrahydrofuran / 2 h / 0 - 20 °C

10.1: o-nitrophenyl selenocyanate; tri-n-butylphosphine / tetrahydrofuran / 1 h / 20 °C

10.2: 95 percent / hydrogen peroxide / tetrahydrofuran; H₂O / 2 h / 0 - 20 °C

11.1: ozone / CH₂Cl₂; methanol / -78 °C

11.2: 92 percent / triphenylphosphine / CH₂Cl₂; methanol / 0.5 h / -78 - 20 °C

12.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -40 °C

12.2: 97 percent / tetrahydrofuran; hexane / 0.5 h / -40 - -20 °C

13.1: tetrahydrofuran / 0.17 h / -78 °C

14.1: NaN(TMS)2 / tetrahydrofuran / 1 h / -78 - -70 °C

14.2: 90 percent / tetrahydrofuran / 1 h / -70 - -60 °C

15.1: 81 percent / n-Bu₃SnH; AIBN / toluene / 2 h / Heating

16.1: 95 percent / aq. HCl / methanol / 1 h / 40 °C

17.1: 90 percent / p-TsOH / benzene / 8 h / Heating

18.1: 85 percent / N,N-bis(salicylidene)ethylenediiminocobalt(II); O₂ / dimethylformamide / 5 h / 20 °C

With piperidine; hydrogenchloride; sodium tetrahydroborate; palladium on activated charcoal; lithium aluminium tetrahydride; n-butyllithium; ortho-nitrophenyl selenocyanate; salcomine; Crabtree's catalyst; 2,2'-azobis(isobutyronitrile); tributylphosphine; hydrogen; oxygen; tri-n-butyl-tin hydride; sodium hexamethyldisilazane; diisobutylaluminium hydride; toluene-4-sulfonic acid; ozone; hydroquinone; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; 1,2-dichloro-benzene; toluene; benzene;
DOI:10.1021/ol016285h

Reference yield:

: 199180-20-6
5,8a-dimethyl-3,4,8,8a-tetrahydro-2H-spiro[naphthalene-1,2′-[1,3]dioxolan]-6(7H)-one

: 363140-03-8
C₂₃H₃₂O₅

Guidance literature:: Multi-step reaction with 17 steps

1.1: H₂; Pd-C; piperidine / 6 h / 20 °C / 7600.51 Torr

1.2: acetic acid / ethanol / 1.5 h / 15 °C

1.3: thionyl chloride; pyridine / CH₂Cl₂ / 1.5 h / 30 °C

2.1: 96 percent / diisobutylaluminum hydride / toluene / 2 h / -78 °C

3.1: 99 percent / sodium borohydride / H₂O; tetrahydrofuran / 0.5 h / 0 °C

4.1: 100 percent / hydrochloric acid / H₂O; methanol / 1 h / 20 °C

5.1: 37 percent / hydroquinone / 1,2-dichloro-benzene / 30 h / 20 - 170 °C

6.1: 96 percent / p-toluenesulfonic acid / benzene / 4 h / Heating

7.1: 77 percent / [Ir(cod)Pcy₃(py)]+PF₆- / CH₂Cl₂ / 48 h / -20 °C

8.1: 100 percent / lithium aluminium hydride / tetrahydrofuran / 2 h / 0 - 20 °C

9.1: o-nitrophenyl selenocyanate; tri-n-butylphosphine / tetrahydrofuran / 1 h / 20 °C

9.2: 95 percent / hydrogen peroxide / tetrahydrofuran; H₂O / 2 h / 0 - 20 °C

10.1: ozone / CH₂Cl₂; methanol / -78 °C

10.2: 92 percent / triphenylphosphine / CH₂Cl₂; methanol / 0.5 h / -78 - 20 °C

11.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -40 °C

11.2: 97 percent / tetrahydrofuran; hexane / 0.5 h / -40 - -20 °C

12.1: tetrahydrofuran / 0.17 h / -78 °C

13.1: NaN(TMS)2 / tetrahydrofuran / 1 h / -78 - -70 °C

13.2: 90 percent / tetrahydrofuran / 1 h / -70 - -60 °C

14.1: 81 percent / n-Bu₃SnH; AIBN / toluene / 2 h / Heating

15.1: 95 percent / aq. HCl / methanol / 1 h / 40 °C

16.1: 90 percent / p-TsOH / benzene / 8 h / Heating

17.1: 85 percent / N,N-bis(salicylidene)ethylenediiminocobalt(II); O₂ / dimethylformamide / 5 h / 20 °C

With piperidine; hydrogenchloride; sodium tetrahydroborate; palladium on activated charcoal; lithium aluminium tetrahydride; n-butyllithium; ortho-nitrophenyl selenocyanate; salcomine; Crabtree's catalyst; 2,2'-azobis(isobutyronitrile); tributylphosphine; hydrogen; oxygen; tri-n-butyl-tin hydride; sodium hexamethyldisilazane; diisobutylaluminium hydride; toluene-4-sulfonic acid; ozone; hydroquinone; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; 1,2-dichloro-benzene; toluene; benzene;
DOI:10.1021/ol016285h