Technology Process of C30H37N5O13
There total 8 articles about C30H37N5O13 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride; water;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/ic402643a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen; 5%-palladium/activated carbon
2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.25 h / 20 °C / Inert atmosphere
2.2: 24.42 h / 20 °C / Inert atmosphere
3.1: hydrogenchloride; water / 1 h / 20 °C / Inert atmosphere
With
hydrogenchloride; 5%-palladium/activated carbon; water; hydrogen; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
DOI:10.1021/ic402643a
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: phosphorus pentabromide / 3 h / 80 °C
2.1: 0.75 h / 0 °C
3.1: potassium phosphate; palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane / 12 h / Reflux
4.1: trifluoroacetic acid / dichloromethane / 20 °C
5.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.25 h / 20 °C / Inert atmosphere
5.2: 24.42 h / 20 °C / Inert atmosphere
6.1: hydrogenchloride; water / 1 h / 20 °C / Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; hydrogenchloride; potassium phosphate; water; palladium diacetate; phosphorus pentabromide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
3.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ic402643a