Technology Process of C21H13F3O
There total 3 articles about C21H13F3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
platinum(II) chloride;
In
toluene;
at 80 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/ol401057z
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trifuran-2-yl-phosphane; tris-(dibenzylideneacetone)dipalladium(0) / toluene / 16 h / 80 °C / Inert atmosphere
2: potassium tert-butylate; dihydrogen peroxide / water; tetrahydrofuran; methanol / 24.5 h / 20 - 65 °C
3: platinum(II) chloride / toluene / 16 h / 80 °C / Inert atmosphere
With
tris-(dibenzylideneacetone)dipalladium(0); trifuran-2-yl-phosphane; potassium tert-butylate; dihydrogen peroxide; platinum(II) chloride;
In
tetrahydrofuran; methanol; water; toluene;
DOI:10.1021/ol401057z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium tert-butylate; dihydrogen peroxide / water; tetrahydrofuran; methanol / 24.5 h / 20 - 65 °C
2: platinum(II) chloride / toluene / 16 h / 80 °C / Inert atmosphere
With
potassium tert-butylate; dihydrogen peroxide; platinum(II) chloride;
In
tetrahydrofuran; methanol; water; toluene;
DOI:10.1021/ol401057z