4-methoxyphenyl (4,6-O-(S)-benzylidene-β-D-galactopyranosyl)-(1->4)-(2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->3)-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:4-methoxyphenyl (4,6-O-(S)-benzylidene-β-D-galactopyranosyl)-(1->4)-(2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->3)-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:1064679-26-0
Molecular Formula:C₈₂H₉₁NO₂₂
Molecular Weight:1442.62
Hs Code.:

4-methoxyphenyl (4,6-O-(S)-benzylidene-β-D-galactopyranosyl)-(1->4)-(2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->3)-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Synonyms:4-methoxyphenyl (4,6-O-(S)-benzylidene-β-D-galactopyranosyl)-(1->4)-(2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->3)-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of 4-methoxyphenyl (4,6-O-(S)-benzylidene-β-D-galactopyranosyl)-(1->4)-(2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->3)-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of 4-methoxyphenyl (4,6-O-(S)-benzylidene-β-D-galactopyranosyl)-(1->4)-(2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->3)-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 1 articles about 4-methoxyphenyl (4,6-O-(S)-benzylidene-β-D-galactopyranosyl)-(1->4)-(2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->3)-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1064679-25-9
4-methoxyphenyl (2,3-di-O-acetyl-4,6-O-(S)-benzylidene-β-D-galactopyranosyl)-(1->4)-(6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->3)-(4-O-acetyl-2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 108-24-7
acetic anhydride

: 1064679-26-0
4-methoxyphenyl (4,6-O-(S)-benzylidene-β-D-galactopyranosyl)-(1->4)-(2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->3)-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: 4-methoxyphenyl (2,3-di-O-acetyl-4,6-O-(S)-benzylidene-β-D-galactopyranosyl)-(1->4)-(6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->3)-(4-O-acetyl-2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside; With hydrazine hydrate; In ethanol; at 80 ℃; for 6h;

acetic anhydride; With pyridine; at 20 ℃; for 6h;

With methanol; sodium methylate; at 20 ℃; for 2h; Further stages.;
DOI:10.1016/j.tet.2008.07.004

Reference yield: 48.0%

: 1064679-26-0
4-methoxyphenyl (4,6-O-(S)-benzylidene-β-D-galactopyranosyl)-(1->4)-(2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->3)-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 155155-64-9
(4S,5R,6R)-4-Acetoxy-5-acetylamino-2-phenylsulfanyl-6-((1S,2R)-1,2,3-triacetoxy-propyl)-tetrahydro-pyran-2-carboxylic acid methyl ester

: C₁₀₂H₁₁₈N₂O₃₄

Guidance literature:: 4-methoxyphenyl (4,6-O-(S)-benzylidene-β-D-galactopyranosyl)-(1->4)-(2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->3)-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside; (4S,5R,6R)-4-Acetoxy-5-acetylamino-2-phenylsulfanyl-6-((1S,2R)-1,2,3-triacetoxy-propyl)-tetrahydro-pyran-2-carboxylic acid methyl ester; With 3 A molecular sieve; In dichloromethane; acetonitrile; at 20 ℃; for 0.5h;

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; acetonitrile; at -10 ℃; for 16h; Further stages.;
DOI:10.1016/j.tet.2008.07.004