5-hydroxy-3-oxo-7-t.butyldiphenylsilyloxy-heptanoic acid α-ethylbenzyl ester

Base Information

Chemical Name:5-hydroxy-3-oxo-7-t.butyldiphenylsilyloxy-heptanoic acid α-ethylbenzyl ester
CAS No.:155504-68-0
Molecular Formula:C₃₂H₄₀O₅Si
Molecular Weight:532.752
Hs Code.:

Synonyms:5-hydroxy-3-oxo-7-t.butyldiphenylsilyloxy-heptanoic acid α-ethylbenzyl ester

Suppliers and Price of 5-hydroxy-3-oxo-7-t.butyldiphenylsilyloxy-heptanoic acid α-ethylbenzyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-hydroxy-3-oxo-7-t.butyldiphenylsilyloxy-heptanoic acid α-ethylbenzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-hydroxy-3-oxo-7-t.butyldiphenylsilyloxy-heptanoic acid α-ethylbenzyl ester

There total 2 articles about 5-hydroxy-3-oxo-7-t.butyldiphenylsilyloxy-heptanoic acid α-ethylbenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 155504-68-0
5-hydroxy-3-oxo-7-t.butyldiphenylsilyloxy-heptanoic acid α-ethylbenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 16 h / Ambient temperature

2: 80 percent / iBu₂AlH / CH₂Cl₂; toluene / 3 h / -70 °C

3: 1.) TiCl₄ / 1.) CH₂Cl₂, -78 deg C, 5 min; 2.) -10/-20 deg C,

With 1H-imidazole; titanium tetrachloride; diisobutylaluminium hydride; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0040-4020(01)85067-5

Reference yield:

: 130442-55-6
3-tert.butyldiphenylsilyloxy-propionitrile

: 155504-68-0
5-hydroxy-3-oxo-7-t.butyldiphenylsilyloxy-heptanoic acid α-ethylbenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / iBu₂AlH / CH₂Cl₂; toluene / 3 h / -70 °C

2: 1.) TiCl₄ / 1.) CH₂Cl₂, -78 deg C, 5 min; 2.) -10/-20 deg C,

With titanium tetrachloride; diisobutylaluminium hydride; In dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)85067-5