Technology Process of C68H62O20
There total 4 articles about C68H62O20 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
-
-
14218-08-7,41881-44-1,53297-33-9,60820-93-1,61198-82-1,67986-91-8,73068-86-7,131897-72-8,131897-73-9
2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl bromide
- Guidance literature:
-
With
4 A molecular sieve; mercury(II) cyanide; mercury dibromide;
In
dichloromethane; acetonitrile;
for 1h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: TsOH / dimethylformamide / 3 h / Ambient temperature
2: 80percent aq. acetic acid / dimethylformamide / 1 h
3: 90 percent / Hg(CN)2, HgBr2, molecular sieves 4 Angstroem / acetonitrile; CH2Cl2 / 1 h
With
4 A molecular sieve; mercury(II) cyanide; toluene-4-sulfonic acid; acetic acid; mercury dibromide;
In
dichloromethane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 80percent aq. acetic acid / dimethylformamide / 1 h
2: 90 percent / Hg(CN)2, HgBr2, molecular sieves 4 Angstroem / acetonitrile; CH2Cl2 / 1 h
With
4 A molecular sieve; mercury(II) cyanide; acetic acid; mercury dibromide;
In
dichloromethane; N,N-dimethyl-formamide; acetonitrile;