9,10-Dibromo-2-tert-butylanthracene

Base Information

• Chemical Name: 9,10-Dibromo-2-tert-butylanthracene
• CAS No.: 114583-08-3
• Molecular Formula: C18H16 Br2
• Molecular Weight: 392.133
• European Community (EC) Number: 662-026-4
• DSSTox Substance ID: DTXSID50399618
• Nikkaji Number: J1.346.197J
• Mol file: 114583-08-3.mol

Synonyms:114583-08-3;9,10-dibromo-2-tert-butylanthracene;9,10-Dibromo-2-(tert-butyl)anthracene;2-TERTBUTYL-9,10-DIBROMOANTHRACENE;2-TERT-BUTYL-9,10-DIBROMOANTHRACENE;SCHEMBL2246981;DTXSID50399618;BWFOVZDGMFZPFX-UHFFFAOYSA-N;2-t-butyl-9,10-dibromoanthracene;2-(t-butyl)-9,10-dibromoanthracene;AKOS024434228;4-cyclohexyl-alpha-methylnaphthalene-1-aceticacid

Chemical Property of 9,10-Dibromo-2-tert-butylanthracene

Chemical Property:

• Vapor Pressure: 4.49E-08mmHg at 25°C
• Refractive Index: 1.668
• Boiling Point: 456.1°Cat760mmHg
• Flash Point: 268.2°C
• PSA: 0.00000
• Density: 1.527g/cm³
• LogP: 6.81550
• XLogP3: 7.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 391.95983
• Heavy Atom Count: 20
• Complexity: 346

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-TERT-BUTYL-9,10-DIBROMOANTHRACENE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)(C)C1=CC2=C(C3=CC=CC=C3C(=C2C=C1)Br)Br

Technology Process of 9,10-Dibromo-2-tert-butylanthracene

There total 1 articles about 9,10-Dibromo-2-tert-butylanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

2-(t-butyl)anthracene (18801-00-8) → 2-tert-butyl-9,10-dibromoanthracene (114583-08-3)

Guidance literature:

With bromine; In tetrachloromethane; at 20 ℃; for 12h;

DOI:10.1039/c2nj20809a

Reference yield: 99.0%

aqueous potassium carbonate + N-bromosuccinamide + 2-(t-butyl)anthracene (18801-00-8) + 2-tert-butyl-9,10-dibromoanthracene (114583-08-3) + phenylboronic acid (98-80-6) → 2-tert-butyl-9,10-diphenylanthracene

Guidance literature:

Pd(PPh₃)4; In N-methyl-acetamide; ethanol; toluene;

Reference yield: 99.0%

aqueous potassium carbonate + N-bromosuccinamide + 2-(t-butyl)anthracene (18801-00-8) + naphthalene-2-boronic acid (32316-92-0) + 2-tert-butyl-9,10-dibromoanthracene (114583-08-3) → 2-tert-butyl-9,10-bis-(β-naphthyl)-anthracene (274905-73-6)

Guidance literature:

Pd(PPh₃)4; In N-methyl-acetamide; ethanol; toluene;

upstream raw materials:

2-(t-butyl)anthracene

Downstream raw materials:

2-tert-butyl-9,10-bis-(β-naphthyl)-anthracene

2-tert-butyl-9,10-bis(2-biphenyl)anthracene