N-Octyl-3-phenylpropenamide

Base Information

• Chemical Name: N-Octyl-3-phenylpropenamide
• CAS No.: 55030-48-3
• Molecular Formula: C₁₇H₂₅NO
• Molecular Weight: 259.392
• Mol file: 55030-48-3.mol

Synonyms:N-octyl-3-phenyl-2-propenamide

Chemical Property of N-Octyl-3-phenylpropenamide

Chemical Property:

• Refractive Index: 1.5200 (estimate)
• Boiling Point: 402.64°C (rough estimate)
• Density: 0.9541 (rough estimate)
• Water Solubility.: 360.6ug/L(temperature not stated)

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-Octyl-3-phenylpropenamide

There total 3 articles about N-Octyl-3-phenylpropenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

n-Octylamine (111-86-4) + cinnamamide (621-79-4) → N-octyl-3-phenyl-2-propenamide (55030-48-3)

Guidance literature:

With Fe³⁺ exchanged montmorillonite K-10; In neat (no solvent); at 140 ℃; for 30h; Inert atmosphere;

DOI:10.1016/j.tetlet.2013.12.111

Reference yield: 88.0%

n-Octylamine (111-86-4) + Cinnamic acid (621-82-9) → N-octyl-3-phenyl-2-propenamide (55030-48-3)

Guidance literature:

Cinnamic acid; With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; at 20 ℃; for 0.0833333h;

n-Octylamine; In dichloromethane; at 20 ℃;

DOI:10.1021/jo102395c

Reference yield:

→ N-octyl-3-phenyl-2-propenamide (55030-48-3)

Guidance literature:

cinnamic anhydride, n-octylamine;

DOI:10.1002/jps.2600571038

upstream raw materials:

n-Octylamine

Cinnamic acid

cinnamamide

Refernces

• 1、 Ayub Ali, Md.,Hakim Siddiki,Kon, Kenichi,Shimizu, Ken-Ichi. "Fe3+-exchanged clay catalyzed transamidation of amides with amines under solvent-free condition". supporting information. p. 1316 - 1319. Retrieved 2014/03/21.
• 2、 Hong,Connors. "Identification of aliphatic amines from rates of cinnamoylation.". . p. 1789 - 1790. Retrieved 2007/10/05.