pentyl {2-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyrimidin-4-yl}carbamate

Base Information

Chemical Name:pentyl {2-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyrimidin-4-yl}carbamate
CAS No.:1192576-17-2
Molecular Formula:C₂₂H₂₆N₆O₃
Molecular Weight:422.487
Hs Code.:

Synonyms:pentyl {2-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyrimidin-4-yl}carbamate

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Chemical Property of pentyl {2-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyrimidin-4-yl}carbamate

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Technology Process of pentyl {2-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyrimidin-4-yl}carbamate

There total 4 articles about pentyl {2-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyrimidin-4-yl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 638-41-5
pentyl chloroformate

: 1192573-89-9
2-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyrimidin-4-amine

: 1192576-17-2
pentyl {2-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyrimidin-4-yl}carbamate

Guidance literature:: With triethylamine; In 1,4-dioxane; at 20 ℃; for 19h;

Reference yield:

: 6919-61-5
N-methoxy-N-methylbenzamide

: 1192576-17-2
pentyl {2-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyrimidin-4-yl}carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethylmagnesium bromide / diethyl ether; dichloromethane / 20 °C

1.2: 0 - 20 °C

2.1: pyridine; hydroxylamine hydrochloride / 75 h / 20 - 50 °C

3.1: caesium carbonate / potassium iodide / N,N-dimethyl-formamide / 101 h / 20 °C

4.1: triethylamine / 1,4-dioxane / 19 h / 20 °C

With pyridine; ethylmagnesium bromide; hydroxylamine hydrochloride; caesium carbonate; triethylamine; potassium iodide; In 1,4-dioxane; diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1192575-99-7
N-hydroxy-1-(1-methyl-1H-imidazol-5-yl)-1-phenylmethanimine

: 1192576-17-2
pentyl {2-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyrimidin-4-yl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / potassium iodide / N,N-dimethyl-formamide / 101 h / 20 °C

2: triethylamine / 1,4-dioxane / 19 h / 20 °C

With caesium carbonate; triethylamine; potassium iodide; In 1,4-dioxane; N,N-dimethyl-formamide;