Technology Process of C25H39BO5Si
There total 8 articles about C25H39BO5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 73 percent / aq. NaOH; Bu4NHSO4 / CH2Cl2
2.1: 98 percent / tetrahydrofuran
3.1: (sia)2BH / tetrahydrofuran
3.2: 97 percent / H2O2; aq. NaOH / tetrahydrofuran
4.1: 100 percent / imidazole / dimethylformamide
5.1: 84 percent / NBS / dimethylformamide
6.1: BuLi / tetrahydrofuran / -78 °C
6.2: tetrahydrofuran / -78 - 0 °C
7.1: aq. HCl
With
1H-imidazole; hydrogenchloride; sodium hydroxide; N-Bromosuccinimide; n-butyllithium; (Sia)2BH; tetra(n-butyl)ammonium hydrogensulfate;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2004-817753
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 100 percent / imidazole / dimethylformamide
2.1: 84 percent / NBS / dimethylformamide
3.1: BuLi / tetrahydrofuran / -78 °C
3.2: tetrahydrofuran / -78 - 0 °C
4.1: aq. HCl
With
1H-imidazole; hydrogenchloride; N-Bromosuccinimide; n-butyllithium;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1055/s-2004-817753
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: (sia)2BH / tetrahydrofuran
1.2: 97 percent / H2O2; aq. NaOH / tetrahydrofuran
2.1: 100 percent / imidazole / dimethylformamide
3.1: 84 percent / NBS / dimethylformamide
4.1: BuLi / tetrahydrofuran / -78 °C
4.2: tetrahydrofuran / -78 - 0 °C
5.1: aq. HCl
With
1H-imidazole; hydrogenchloride; N-Bromosuccinimide; n-butyllithium; (Sia)2BH;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1055/s-2004-817753