(3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-glucofuranos-3-yl) (methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranosid-6-yl) selenide

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Chemical Name:(3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-glucofuranos-3-yl) (methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranosid-6-yl) selenide
CAS No.:1221269-56-2
Molecular Formula:C₄₀H₅₀O₁₀Se
Molecular Weight:769.791
Hs Code.:

Synonyms:(3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-glucofuranos-3-yl) (methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranosid-6-yl) selenide

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Chemical Property of (3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-glucofuranos-3-yl) (methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranosid-6-yl) selenide

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Technology Process of (3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-glucofuranos-3-yl) (methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranosid-6-yl) selenide

There total 1 articles about (3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-glucofuranos-3-yl) (methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranosid-6-yl) selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 55951-90-1
1,2:5,6-di-O-isopropylidene-3-O-trifluoromethanesulfonyl-α-D-allofuranose

: 1221269-54-0
bis(methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranosid-6-yl) diselenide

: 1221269-56-2
(3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-glucofuranos-3-yl) (methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranosid-6-yl) selenide

Guidance literature:: bis(methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranosid-6-yl) diselenide; With sodium tetrahydroborate; In N,N-dimethyl-formamide; at 50 ℃; for 0.5h; Inert atmosphere;

1,2:5,6-di-O-isopropylidene-3-O-trifluoromethanesulfonyl-α-D-allofuranose; In N,N-dimethyl-formamide; at 50 ℃; for 15h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.02.064