3-methoxy-bisaniline

Base Information

Chemical Name:3-methoxy-bisaniline
CAS No.:119703-28-5
Molecular Formula:C₁₃H₂₁NO₃
Molecular Weight:239.315
Hs Code.:

3-methoxy-bis<N,N-(2-methoxyethyl)>aniline

Synonyms:3-methoxy-bisaniline

Suppliers and Price of 3-methoxy-bisaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methoxy-bisaniline

Chemical Property:

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Technology Process of 3-methoxy-bisaniline

There total 3 articles about 3-methoxy-bisaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 17126-75-9
3-methoxy-bisaniline

: 77-78-1
dimethyl sulfate

: 119703-28-5
3-methoxy-bisaniline

Guidance literature:: With potassium hydroxide; parafffin oil; sodium hydride; In toluene; 1.) reflux, 2 h; 2.) rt.;
DOI:10.1016/S0022-1139(00)82776-1

Reference yield: 83.0%

: 536-90-3,918666-97-4
m-Anisidine

: 6482-24-2
2-Bromoethyl methyl ether

: 119703-28-5
3-methoxy-bisaniline

Guidance literature:: With potassium carbonate; In acetonitrile; at 80 ℃; for 24h; Inert atmosphere;

Reference yield:

: 536-90-3,918666-97-4
m-Anisidine

: 119703-28-5
3-methoxy-bisaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / water / 45 h, rt., then 1 h, 70 deg C

2: 94 percent / 1.) 80percent sodium hydride/parafffin oil; 2.) 50percent aq. potassium hydroxide / toluene / 1.) reflux, 2 h; 2.) rt.

With potassium hydroxide; parafffin oil; water; sodium hydride; In toluene;
DOI:10.1016/S0022-1139(00)82776-1