6-(2-Nitrophenoxy)-1H,3H-naphtho[1,8-cd]pyran-1,3-dione

Base Information

Chemical Name:6-(2-Nitrophenoxy)-1H,3H-naphtho[1,8-cd]pyran-1,3-dione
CAS No.:111669-59-1
Molecular Formula:C₁₈H₉NO₆
Molecular Weight:335.273
Hs Code.:
European Community (EC) Number:601-108-6
DSSTox Substance ID:DTXSID301203234
Nikkaji Number:J2.972.070C

Synonyms:SCHEMBL16684654;WVAKQJWUJQLVEN-UHFFFAOYSA-N;DTXSID301203234;111669-59-1;6-(2-Nitrophenoxy)-1H,3H-naphtho[1,8-cd]pyran-1,3-dione

Suppliers and Price of 6-(2-Nitrophenoxy)-1H,3H-naphtho[1,8-cd]pyran-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(2-Nitrophenoxy)-1H,3H-naphtho[1,8-cd]pyran-1,3-dione

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:335.04298701
Heavy Atom Count:25
Complexity:572

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)[N+](=O)[O-])OC2=C3C=CC=C4C3=C(C=C2)C(=O)OC4=O

Technology Process of 6-(2-Nitrophenoxy)-1H,3H-naphtho[1,8-cd]pyran-1,3-dione

There total 3 articles about 6-(2-Nitrophenoxy)-1H,3H-naphtho[1,8-cd]pyran-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 81-86-7
4-bromo-1,8-naphthalenedicarboxylic anhydride

: 88-75-5,78813-12-4
2-hydroxynitrobenzene

: 111669-59-1
4-(2-Nitrophenoxy)-1,8-naphthalic anhydride

Guidance literature:: With copper; sodium hydroxide; In N,N-dimethyl-formamide; for 1h; Reflux;
DOI:10.1016/j.ejmech.2011.04.040

Reference yield: 82.0%

: 4053-08-1
p-chloro-1,8-naphthalicanhydride

: 88-75-5,78813-12-4
2-hydroxynitrobenzene

: 111669-59-1
4-(2-Nitrophenoxy)-1,8-naphthalic anhydride

Guidance literature:: With sodium hydroxide; copper; In N,N-dimethyl-formamide; for 1h; Heating;

Reference yield:

: 81-84-5
1,8-Naphthalic anhydride

: 111669-59-1
4-(2-Nitrophenoxy)-1,8-naphthalic anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 85percent H₃PO₄, aq. NaOH, Cl₂ / 3 h / Ambient temperature

2: 71 percent / KOH, Cu / dimethylformamide / 1 h / Heating

With potassium hydroxide; sodium hydroxide; phosphoric acid; chlorine; copper; In N,N-dimethyl-formamide;
DOI:10.1021/je00054a038