C₃₁H₃₇BN₂O₉

Base Information

Chemical Name:C₃₁H₃₇BN₂O₉
CAS No.:1379654-47-3
Molecular Formula:C₃₁H₃₇BN₂O₉
Molecular Weight:592.454
Hs Code.:

C<sub>31</sub>H<sub>37</sub>BN<sub>2</sub>O<sub>9</sub>

Synonyms:C₃₁H₃₇BN₂O₉

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Chemical Property of C₃₁H₃₇BN₂O₉

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Technology Process of C₃₁H₃₇BN₂O₉

There total 6 articles about C₃₁H₃₇BN₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1379654-46-2
C₂₁H₂₆BNO₇

: 3417-91-2
L-tyrosine methyl ester HCl

: 1379654-47-3
C₃₁H₃₇BN₂O₉

Guidance literature:: C₂₁H₂₆BNO₇; L-tyrosine methyl ester HCl; With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In chloroform; at 0 ℃; for 1h;

In chloroform; at 20 ℃; for 24h;
DOI:10.1002/chem.201103185

Reference yield:

: 691394-91-9
methyl (S)-3-(4-(benzyloxy)-3-iodophenyl)-2-((tert-butoxycarbonyl)amino)propanoate

: 1379654-47-3
C₃₁H₃₇BN₂O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / dimethyl sulfoxide / 20 h / 80 °C / Inert atmosphere

2.1: sodium periodate; ammonium acetate; water / acetone / 17 h / 20 °C

3.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol / 1 h / 0 °C

3.2: 1 h / 20 °C

4.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 1 h / 0 °C

4.2: 24 h / 20 °C

With sodium periodate; 1-hydroxy-7-aza-benzotriazole; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; lithium hydroxide monohydrate; ammonium acetate; water; potassium acetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; chloroform; dimethyl sulfoxide; acetone;
DOI:10.1002/chem.201103185

Reference yield:

: 1338925-50-0
(S)-O-benzyl-N-tert-butoxycarbonyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)tyrosine methyl ester

: 1379654-47-3
C₃₁H₃₇BN₂O₉

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium periodate; ammonium acetate; water / acetone / 17 h / 20 °C

2.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol / 1 h / 0 °C

2.2: 1 h / 20 °C

3.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 1 h / 0 °C

3.2: 24 h / 20 °C

With sodium periodate; 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; ammonium acetate; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; chloroform; acetone;
DOI:10.1002/chem.201103185