1--3-propane

Base Information

Chemical Name:1--3-propane
CAS No.:154220-33-4
Molecular Formula:C₃₇H₅₃N₅O₆S₃
Molecular Weight:760.056
Hs Code.:

1-<N,N'-bis(p-toluenesulfonyl)-1,4,7-triaza-1-cyclononyl>-3-<N-(p-toluenesulfonyl)-1,4-diaza-1-cyclononyl>propane

Synonyms:1--3-propane

Suppliers and Price of 1--3-propane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1--3-propane

Chemical Property:

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Technology Process of 1--3-propane

There total 7 articles about 1--3-propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 154220-29-8
N-(p-toluenesulfonyl)-1,4-diazacyclononane

: 154220-31-2
1--3-chloropropane

: 154220-33-4
1--3-propane

Guidance literature:: With triethylamine; sodium iodide; In acetonitrile; for 24h; Heating;
DOI:10.1016/S0040-4020(01)81895-0

Reference yield:

: 111-24-0
1,5-dibromo-pentane

: 154220-33-4
1--3-propane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, 90 deg C, 1 h, 2.) DMF, 90 deg C, 24 h

2: 93 percent / 1.) conc. H₂SO₄, 2.) 15 N NaOH / 48 h / 90 °C

3: 72 percent / 7.5 N NaOH / diethyl ether / 3 h / Ambient temperature

4: 70 percent / sodium iodide, triethylamine / acetonitrile / 24 h / Heating

With sodium hydroxide; sulfuric acid; sodium hydride; triethylamine; sodium iodide; In diethyl ether; acetonitrile;
DOI:10.1016/S0040-4020(01)81895-0

Reference yield:

: 95388-08-2
N,N'-bis(p-toluenesulfonyl)-1,4,7-triazacyclononane

: 154220-33-4
1--3-propane

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / triethylamine / acetonitrile / 18 h / Heating

2: 70 percent / sodium iodide, triethylamine / acetonitrile / 24 h / Heating

With triethylamine; sodium iodide; In acetonitrile;
DOI:10.1016/S0040-4020(01)81895-0