2-(2-bromophenyl)-2-methylpropionaldehyde

Base Information

Chemical Name:2-(2-bromophenyl)-2-methylpropionaldehyde
CAS No.:212626-89-6
Molecular Formula:C₁₀H₁₁BrO
Molecular Weight:227.101
Hs Code.:

Synonyms:2-(2-bromophenyl)-2-methylpropionaldehyde

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Chemical Property of 2-(2-bromophenyl)-2-methylpropionaldehyde

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Technology Process of 2-(2-bromophenyl)-2-methylpropionaldehyde

There total 3 articles about 2-(2-bromophenyl)-2-methylpropionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 57775-06-1
2-(2-bromophenyl)-2-methylpropanenitrile

: 212626-89-6
2-(2-bromophenyl)-2-methylpropionaldehyde

Guidance literature:: With diisobutylaluminium hydride; In hexane; toluene; 1.) -70 deg C, 30 min, 2.) room temperature, 1 h;
DOI:10.1021/jo980697v

Reference yield:

: 177748-64-0
2-(2-bromophenyl)-2-methylpropan-1-ol

: 212626-89-6
2-(2-bromophenyl)-2-methylpropionaldehyde

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1021/jacs.8b02761

Reference yield:

: 177748-63-9
methyl 2-(2-bromophenyl)-2-methylpropanoate

: 212626-89-6
2-(2-bromophenyl)-2-methylpropionaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 - -25 °C

2: pyridinium chlorochromate / dichloromethane / 3 h / 0 - 20 °C

With diisobutylaluminium hydride; pyridinium chlorochromate; In dichloromethane; toluene;
DOI:10.1021/jacs.8b02761